Skip to main content
SpringerLink
Log in

LC Determination of Nosiheptide in Swine Kidney and Liver

  • Full Short Communication
  • Published:
Chromatographia Aims and scope Submit manuscript

Abstract

A liquid chromatographic method was developed for determination of nosiheptide in swine kidney and liver. The tissue samples were extracted with acetonitrile and defatted with hexane. The analytes were determined at a fluorescence excitation/emission wavelength of 357/515 nm and with gradient elution program. The limits of detection and limits of quantification were 5 and 20 ng g−1, respectively, for swine kidney and liver. The mean recoveries for nosiheptide in swine kidney and liver ranged from 70.3 to 97.4% with coefficients of variation below 11.3% at 20–100 ng g−1 fortification levels.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2

References

  1. Tanaka T, Endo T, Shimazu A (1970) J Antibiot 23:231–237

    CAS  Google Scholar 

  2. Prange T, Ducruix A, Pascard C, Lunel J (1977) Nature 265:189–190

    Article  CAS  Google Scholar 

  3. Benazet F, Cartier M, Florent J, Godard C, Jung G, Lunel J, Mancy D, Pascal C, Renaut J, Tarridec P, Theilleux J, Tissier R, Dubost M, Ninet L (1980) Experientia 36(4):414–416

    Article  CAS  Google Scholar 

  4. Tanaka T, Sakaguchi K, Yonehara H (1970) J Antibiot 23:401–407

    CAS  Google Scholar 

  5. Tanaka T, Sakaguchi K, Yonehara H (1971) J Antibiot 24:537–542

    CAS  Google Scholar 

  6. Krinke AL, Jamroz D (1996) Poult Sci 75:705–710

    CAS  Google Scholar 

  7. Cundliffe E, Thompson J (1981) J Gen Microbiol 126:185–192

    CAS  Google Scholar 

  8. Wu T, Huang H, Zhou P (1997) Chin J Antibiot 6:373–376

    Google Scholar 

  9. Cromwell GL, Stahly TS, Speer VC, O’Kelly R (1984) J Anim Sci 59:1125–1128

    CAS  Google Scholar 

  10. Wu XL (2005) Feed Industry 6:53–56

    Google Scholar 

  11. Li HJ, Zhou XT (2005) Chin J Vet Sci 25:534–535

    CAS  Google Scholar 

  12. Noh SH, Moon HK, Han IK, Shin IS (1995) Han’guk Ch’uksan Hakhoechi 37:66–72

    CAS  Google Scholar 

  13. Maximum Residue Limits (MRLs) for Agricultural Chemicals in Foods of Japan. http://www.mhlw.go.jp/english/topics/mrls/mrls.html

  14. Li X, Wu PL, Lin WB (1999) Chin J Pharm Ind 30:548–550

    Google Scholar 

  15. The Executive Commission of the Chinese Pharmacopoeia Commission (2005) Chinese Pharmacopoeia Publication House of Chemical Industry: Beijing, China, pp 81–84

  16. Yamatani S, Akimoto K (1997) Shiryo Kenkyu Hokoku 22:116–125

    CAS  Google Scholar 

  17. Akimoto K, Fukumoto Y (1995) Shiryo Kenkyu Hokoku 20:81–93

    CAS  Google Scholar 

  18. Fukumoto Y (1992) Shiryo Kenkyu Hokoku 17:72–80

    CAS  Google Scholar 

  19. Kusama T, Yamatani S (1988) Chikusan no Kenkyu 42:371–374

    CAS  Google Scholar 

  20. Claude P, Claude G, Marie M (1979) J Assoc Off Anal Chem 62:976–981

    Google Scholar 

  21. Liu L (1996) Chin J Pharm Ind 27:453–455

    Google Scholar 

  22. Hidekazu S (1990) Shiryo Kenkyu Hokoku 15:67–80

    Google Scholar 

  23. Yamamoto Y, Sonoda E, Ono K, Takeda O (1992) Miyazaki Ken Eisei Kankyo Kenkyusho Nerpo 3:50–53

    Google Scholar 

  24. Shozo H, Naoto O (2000) J AOAC Int 83:17–19

    Google Scholar 

Download references

Acknowledgment

This work was supported by the Program for New Century Excellent Talents in University (No. NCET-08-0538) and the National Key Technologies Research and Development Program of China during the 11th Five-Year Plan Period (No. 2006BAD31B08).

Author information

Authors and Affiliations

  1. Department of Pharmacology and Toxicology, College of Veterinary Medicine, China Agricultural University, 100193, Beijing, People’s Republic of China

    Haiyang Jiang , Xi Xia, Shuangyang Ding, Fei Xu, Jianzhong Shen, Xiaowei Li & Jinfeng Liu

  2. National Reference Laboratory for Veterinary Drug Residue, 100193, Beijing, People’s Republic of China

    Haiyang Jiang , Xi Xia, Shuangyang Ding, Jianzhong Shen, Xiaowei Li & Jinfeng Liu

  3. Qinghai Animal Husbandry & Veterinary College, 812100, Huangyuan, People’s Republic of China

    Weihong Zhai

Authors
  1. Haiyang Jiang
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Weihong Zhai
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Xi Xia
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Shuangyang Ding
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Fei Xu
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Jianzhong Shen
    View author publications

    You can also search for this author in PubMed Google Scholar

  7. Xiaowei Li
    View author publications

    You can also search for this author in PubMed Google Scholar

  8. Jinfeng Liu
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Jianzhong Shen.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Jiang , H., Zhai, W., Xia, X. et al. LC Determination of Nosiheptide in Swine Kidney and Liver. Chroma 71, 131–134 (2010). https://doi.org/10.1365/s10337-009-1418-z

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1365/s10337-009-1418-z

Keywords

Search

Navigation