Skip to main content
SpringerLink
Log in

Determination of Six Resorcylic Acid Lactones in Feed by GC–MS

  • Limited Short Communication
  • Published:
Chromatographia Aims and scope Submit manuscript

Abstract

A method was developed to simultaneously detect six resorcylic acid lactones in feed by GC–MS. Samples were extracted with methanol followed by a two step liquid–liquid extraction and an HLB SPE clean-up. The samples were derivatized with BSTFA + TMCS (99/1; v/v) and determined by GC–MS. For all analytes, the ranges of recoveries were 81.2–98.2%, with RSDs of 3.2–15.2%, and the LODs were 0.2–0.6 μg kg−1.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1

References

  1. Blokland MH, Sterk SS, Stephany RW, Launay FM, Kennedy DG, Ginkel L (2006) Anal Bioanal Chem 384:1221–1227

    Article  CAS  Google Scholar 

  2. Güzin ÖB, Hilal K, Sefa Ç, Nil Ü, Mert P, Tevhide S (2007) Ankara Univ Hekim Fak Derg 54:7–10

    Google Scholar 

  3. Takasumi K, Kosaku T, Hideyuki M, Kensuke N (2009) Biosci Biotechnol Biochem 73:1118–1122

    Article  Google Scholar 

  4. Wang S, Wang XH (2007) Food Addit Contam 24:573–582

    Article  CAS  Google Scholar 

  5. Wei Z, Hejia W, Jianping W, Xiaowei Li, Haiyang J, Jianzhong S (2006) J AOAC Int 89:1677–1681

    Google Scholar 

  6. Marchand P, le Bizec B, Gade C, Monteau F, André F (2000) J Chromatogr A 867:219–233

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Institute of Veterinary Medicine, China Agricultural University, Beijing, 100193, China

    Jianzhong Shen, Suxia Zhang, Congming Wu, Haiyang Jiang, Zhanhui Wang & Linli Cheng

Authors
  1. Jianzhong Shen
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Suxia Zhang
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Congming Wu
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Haiyang Jiang
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Zhanhui Wang
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Linli Cheng
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Linli Cheng.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Shen, J., Zhang, S., Wu, C. et al. Determination of Six Resorcylic Acid Lactones in Feed by GC–MS. Chroma 71, 163–165 (2010). https://doi.org/10.1365/s10337-009-1399-y

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1365/s10337-009-1399-y

Keywords

Search

Navigation