Skip to main content
SpringerLink
Log in

Quantitative Analysis of Caffeoylquinic Acids and Styrylpyrones in Sweetia panamensis Bark by UPLC

  • Original
  • Published:
Chromatographia Aims and scope Submit manuscript

Abstract

Six secondary metabolites from the methanolic extract of Sweetia panamensis (Fabaceae) bark were isolated and characterised. Along with the pyrones desmethylangonine β-d-O-glucopyranoside and desmethylangonine β-d-O-glucopyranosyl-(1→6)-O-β-d-glucopyranoside, already reported in this species, 5-O-caffeoylquinic acid (chlorogenic acid), 4-O-caffeoylquinic acid, 3-O-caffeoylquinic acid and the isoflavonoid 5-O-methylgenistein 7-O-β-d-glucopyranoside were isolated for the first time from S. panamensis. Additionally, an LC-ESI-MS qualitative analysis was performed and an ultra performance liquid chromatography (UPLC) method was developed and validated for the determination of these compounds. The UPLC method was applied to the quantitative analysis of plant samples. Pyrones and caffeoylquinic acids resulted to be the main compounds in the extract; in particular desmethylangonine β-d-O-glucopyranosyl-(1→6)-O-β-d-glucopyranoside was the most abundant compound.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3

Similar content being viewed by others

References

  1. Andrade-Cetto A, Heinrich M (2005) J Ethnopharmacol 99:325–348

    Article  Google Scholar 

  2. Nuzillard JM, Connolly JD, Delaude C, Richard B, Zèches-Hanrot M, Le Men-Olivier L (1999) Tetrahedron 55:11511–11518

    Article  CAS  Google Scholar 

  3. Veitch NC, Goodwin BL, Kite GC, Simmonds MSJ (1997) Phytochem 45:847–850

    Article  CAS  Google Scholar 

  4. Andrade-Cetto A, Wiedenfeld H (2004) J Ethnopharmacol 90:217–220

    Article  Google Scholar 

  5. Jiang TF, Wang YH, Lv ZH, Yue ME (2007) J Pharm Biomed Anal 43:854–858

    Article  CAS  Google Scholar 

  6. Choi YH, Kim HK, Linthorst HJM, Hollander JG, Lefeber AWM, Erkelens C, Nuzillard JM, Verpoorte R (2006) J Nat Prod 69:742–748

    Article  CAS  Google Scholar 

  7. Guang Ma W, Fukushi Y, Hostettmenn K, Tahara S (1998) Phytochem 49:251–254

    Article  Google Scholar 

  8. Wiedenfeld H, Andrade-Cetto (2003) J Biosci 58:637–639

  9. Xiaoqin L, Zhili X, Xixiang Y, Lanchong C, Wenliang Z, Famei L (2006) Anal Chim Acta 580:170–180

    Article  Google Scholar 

  10. De Villiers A, Lestremau F, Szucs R, Gélébart S, David F, Sandra P (2006) J Chromatogr A 1127:60–69

    Article  Google Scholar 

  11. ICH Q2B (1995), International Conference on Harmonisation, London, 1995

Download references

Author information

Authors and Affiliations

  1. Dipartimento di Scienze Farmaceutiche, Università di Salerno, Via ponte don Melillo, 84084, Fisciano (SA), Italy

    Mariateresa Maldini, Paola Montoro, Sonia Piacente & Cosimo Pizza

  2. Department of Biochemistry, Institute of Soil Science and Plant Cultivation, ul. Czartoryskich 8, 24-100, Puławy, Poland

    Ireneusz Kapusta & Wieslaw Oleszek

Authors
  1. Mariateresa Maldini
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Paola Montoro
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Ireneusz Kapusta
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Wieslaw Oleszek
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Sonia Piacente
    View author publications

    You can also search for this author in PubMed Google Scholar

  6. Cosimo Pizza
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Cosimo Pizza.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Maldini, M., Montoro, P., Kapusta, I. et al. Quantitative Analysis of Caffeoylquinic Acids and Styrylpyrones in Sweetia panamensis Bark by UPLC. Chroma 70, 1621–1626 (2009). https://doi.org/10.1365/s10337-009-1376-5

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1365/s10337-009-1376-5

Keywords

Search

Navigation