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Analysis of Para Red and Sudan Dyes in Egg Yolk by UPLC–MS–MS

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Abstract

Matrix solid-phase dispersion (MSPD) with alumina N as adsorbent has been used for extraction of para red, Sudan 1, Sudan 2, Sudan 3, and Sudan 4 dyes from egg yolk. The extracts were analyzed by ultra-performance liquid chromatography–tandem mass spectrometry (UPLC–MS–MS). Mean recovery for the five dyes ranged from 63.2 to 98.6%, with CV 0.55–10.00%. One sample was confirmed to contain 0.3 mg kg−1 Sudan 4.

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Acknowledgments

This research was financially supported by Beijing Municipal Natural Science Foundation (7082065) and the National High-tech Research, Development Project (2007AA06Z404) of China and Beijing key lab. of TCVM.

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Authors and Affiliations

  1. Department of Animal Science, Beijing University of Agriculture, 102206, Beijing, China

    Xiaolin Hou & Zhongwen Zhang

  2. Circulation Industry Promotion Center, Ministry of Business, 100070, Beijing, China

    Yonggang Li

  3. Department of Animal Science, Beijing Vocational College of Agriculture, 102442, Beijing, China

    Shoujun Cao

  4. Institute of Nutrition and Food Hygiene, Chinese Center for Disease Control and Prevention, 100050, Beijing, China

    Yongnin Wu

Authors
  1. Xiaolin Hou
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  2. Yonggang Li
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  3. Shoujun Cao
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  4. Zhongwen Zhang
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  5. Yongnin Wu
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Corresponding authors

Correspondence to Zhongwen Zhang or Yongnin Wu.

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Hou, X., Li, Y., Cao, S. et al. Analysis of Para Red and Sudan Dyes in Egg Yolk by UPLC–MS–MS. Chroma 71, 135–138 (2010). https://doi.org/10.1365/s10337-009-1357-8

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