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An LC–DAD Fingerprinting Method for Alkaloids, Flavonoids and Styrylpyrones from Cryptocarya mandioccana

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Abstract

An LC–DAD method has been developed in order to evaluate qualitatively and quantitatively quaternary aporphine alkaloids, flavonoid glycosides and styrylpyrones, which are the main secondary metabolites of leaves from C. mandioccana. The chromatographic method was validated considering both internal and external standard quantification methods and showed good performances in terms of selectivity, linearity, precision (repeatability and intermediate precision), limit of detection, limit of quantification, accuracy and stability.

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Acknowledgments

The authors are grateful to Biota-FAPESP for financial support, and to CNPq for the Ph.D. scholarship granted to Karin Fabiana Bandeira. We would also like to acknowledge the Instituto Florestal de São Paulo for authorizing the collection of C. mandioccana samples at the Carlos Botelho State Park.

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Authors and Affiliations

  1. Institute of Chemistry, Nucleus of Bioassay, Biosynthesis and Ecophysiology of Natural Products, NuBBE, São Paulo State University, UNESP, CEP 14801-970, Araraquara, SP, 355, Brazil

    Karin F. Bandeira & Alberto José Cavalheiro

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  1. Karin F. Bandeira
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  2. Alberto José Cavalheiro
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Correspondence to Alberto José Cavalheiro.

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Bandeira, K.F., Cavalheiro, A.J. An LC–DAD Fingerprinting Method for Alkaloids, Flavonoids and Styrylpyrones from Cryptocarya mandioccana . Chroma 70, 1455–1460 (2009). https://doi.org/10.1365/s10337-009-1338-y

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  • DOI: https://doi.org/10.1365/s10337-009-1338-y

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