Abstract
A newly modified extractor facilitated rapid extraction (10.0 mL, 1 h) of eleven phenols from XAD-4 resin for comparable recoveries to those with conventional Soxhlet extractor (80.0 mL, 3 h). Combined with analysis by gas chromatography and gas chromatography-mass spectrometry in selected ion monitoring mode as tert-butyldimethylsilyl derivatives, the overall method was linear (≥ 0.9991) with satisfactory precision (≤ 9.2% RSD), accuracy (≤ 7.7% RE), detection limit (≤ 0.02 μg L−1), and recovery rates (≥ 75.0%) in 0.05 to 1.0 μg L−1. Six phenolic pollutants were quantitatively screened along with bisphenol A (0.028 μg L−1) from river water.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
References
Masque N, Pocurull E, Marce RM, Borrull F (1998) Chromatographia 47:176–182
Castillo M, Barcelo D, Pereira AS, Aquino Neto FR (1999) Trends in Anal Chem 18:26–36
Corce V, Patrolecco L, Polesello S, Valsecchi S (2003) Chromatographia 58:145–149
Helaleh MIH, Takabayashi Y, Fujii S, Korenaga T (2001) Anal Chim Acta 428:227–234
Lagana A, Bacaloni A, Leva ID, Faberi A, Fago G, Marino A (2004) Anal Chim Acta 501:79–88
Rodriguez I, Llompart MP, Cela R (2000) J Chromatogr A 885:291–304
Bruzzoniti MC, Sarzanini C, Mentasti E (2000) J Chromatogr A 902:289–309
Galceran MT, Jauregui O (1995) Anal Chim Acta 304:75–84
Pocurull E, Sanchez G, Borrull F, Marce RM (1995) J Chromatogr A 696:31–39
Pocurrull E, Calull M, Marce RM, Borrull F (1996) J Chromatogr A 719:105–112
Puig D, Barcelo D (1996) J Chromatogr A 733:371–381
Crespin MA, Ballesteros E, Gallego M, Valcarcel M (1997) J Chromatogr A 757:165–172
Cheung J, Wells RJ (1997) J Chromatogr A 771:203–211
Rodriguez I, Mejuto MC, Bollain MH, Cela R (1997) J Chromatogr A 786:285–292
Heberer T, Stan HJ (1997) Anal Chim Acta 341:21–34
Luz EVA, Jose LGP, Evangelina CF (1999) Talanta 50:509–526
Di Corcia A, Marchese S, Samperi R (1993) J Chromatogr 642:175–184
Di Corcia A, Bellini A, Madbouly MD, Marchese S (1996) J Chromatogr A 733:383–393
Gesssler A, Schoeler HF (1994) Wat Res 28:2047–2058
Kim KR, Kim H (2000) J Chromatogr A 866:87–96
Kim H, Hong JK, Kim YH, Kim KR (2003) Arch Pharm Res 26:697–705
Acknowledgments.
This study was supported in part by the Ministry of Environment (Korea Environmental Research and development Fund, 1998) and in part by the Brain Korea 21 Project in 2003.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Paik, M., Park, J., Koo, W. et al. Modification of Soxhlet Extractor for Rapid and Effective Recovery of Phenolic Pollutants Adsorbed on XAD-4 Resin. Chromatographia 60, 693–698 (2004). https://doi.org/10.1365/s10337-004-0444-0
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1365/s10337-004-0444-0