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Preparation and Evaluation of Mono (6A-N-Ethylenediamine-6A-Deoxy)-Functionalized β-Cyclodextrin Bonded Stationary Phases for Normal and Reverse-Phase High-Performance Liquid Chromatography

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Abstract

The preparation, characterization and potential liquid chromatographic applications of two totally and partly functionalized β-cyclodextrin-bonded stationary phases were presented. Separation of a series of organophosphorus racemic compounds was achieved under normal and reverse-phase conditions. Separation factor was up to 1.812 and resolution up to 4.072. The influence of chromatographic conditions was investigated and the possible chiral recognition mechanism was proposed.

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References

  • Armstrong DW, Stalcup AM, Hilton ML, Duncan JD, Faulkner JR, Jr, Chang S-C (1990) Anal Chem 62:1610–1615

    CAS  Google Scholar 

  • Nakamura K, Fujima H, Kitagawa H, Wada H, Makino K (1995) J Chromatogr A 694:111–118

    Article  CAS  Google Scholar 

  • Zhang LF, Wong YC, Chen L, Ching CB, Ng SC (1999) Tetrahedron Lett 40:1815–1818

    Article  CAS  Google Scholar 

  • Zhang LF, Chen L, Lee TC, Ng SC (1999) Tetrahedron:Asymmetry 10:4107–4113

    Google Scholar 

  • Lai XH, Ng SC (2003) Tetrahedron Lett 44:2657–2660

    Article  CAS  Google Scholar 

  • Chen H, Lv XY, Gao RY, Wang QS (1999) Chinese J Chem 17(6):644–649

    CAS  Google Scholar 

  • Chen H, Lv XY, Gao RY, Zhou J, Wang QS (2000) Chinese J Chem 18(4):533–536

    CAS  Google Scholar 

  • Huang JM, Chen H, Wang QS, Gao RY, Chen RY (2001) Acta Chimica Sinica 59(8):1299–1305

    CAS  Google Scholar 

  • Huang JM, Chen H, Wang QS, Gao RY, Chen RY (2001) Acta Chimica Sinica 59(11):1975–1981

    CAS  Google Scholar 

  • Chen H, Lv XY, Huang JM, Gao RY, Wang QS (2000) Chemical J Chinese Universities 21(4):562–565

    CAS  Google Scholar 

  • Chen H, Lv XY, Gao RY, Wang QS (2000) Chemical J Chinese Universities 21(2):233–236

    CAS  Google Scholar 

  • Huang JM, Chen H, Gao RY, Wang QS (2001) Chemical J Chinese Universities 22(11):1838–1842

    CAS  Google Scholar 

  • Zhou AL, Wang XL, Huang JM, Gao RY (2003) Chemical J Chinese Universities 9:1610–1614

    Google Scholar 

  • Vizitin D, Walkinshaw CS, Gorin BI, Thatcher GRI (1997) J Org Chem 62:8760–8766

    Article  Google Scholar 

  • Li B (2000) Doctor Dissertation. Chem Dept Nankai Univ Tian Jin [D],

  • Zhou AL, Lv XY, Huang JM, Wang XS, Gao RY (2002) Chinese J Chromatogr 20(6):502–507

    CAS  Google Scholar 

Download references

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Authors and Affiliations

  1. State Key Laboratory of Elemento-Organic Chemistry, Nankai University, Tianjin, 300071, P.R.China

    A. L. Zhou, H. X. Wang & R. Y. Gao

  2. College of Chemistry, Nankai University, Tianjin, 300071, P.R.China

    X. S. Wang

  3. College of Life Science, Nankai University, Tianjin, 300071, P.R.China

    X. Y. Lv, Y. X. Xie & G. Q. Liu

Authors
  1. A. L. Zhou
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  2. X. Y. Lv
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  3. Y. X. Xie
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  4. G. Q. Liu
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  5. H. X. Wang
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  6. X. S. Wang
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  7. R. Y. Gao
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Corresponding author

Correspondence to R. Y. Gao.

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Zhou, A., Lv, X., Xie, Y. et al. Preparation and Evaluation of Mono (6A-N-Ethylenediamine-6A-Deoxy)-Functionalized β-Cyclodextrin Bonded Stationary Phases for Normal and Reverse-Phase High-Performance Liquid Chromatography. Chromatographia 60, 281–285 (2004). https://doi.org/10.1365/s10337-004-0342-5

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  • DOI: https://doi.org/10.1365/s10337-004-0342-5

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