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Synthesis and Investigation of the Properties of Al2O3–Y2O3 Powders Using Nanospray Drying

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Abstract

We isolated Al2O3–Y2O3 powders using two different methods: filtration and nanospray drying. The obtained samples were investigated using thermogravimetry, differential scanning calorimetry, X-ray phase analysis, BET, and scanning electron microscopy. We examined the processes of linear shrinkage during thermal and compression consolidation using field-assisted sintering. A comparative analysis of the powders obtained by the two methods was conducted and the results are presented and discussed. A powder containing 96 vol % of the Y3Al5O12 phase can be produced through calcination of the precursor obtained by nanospray drying at 1100°C for 10 min.

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Funding

The work was supported by the State tasks Science (BCh) (no. FSWW-2023-0011) using the equipment of the Center for Sharing Use “Nanomaterials and Nanotechnologies” TPU, supported by the RF Ministry of Science and Higher Education (project no. 075-15-2021-710).

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Authors and Affiliations

  1. Tomsk Polytechnic University, 634050, Tomsk, Russia

    V. D. Paigin, D. E. Deulina, A. E. Ilela, G. V. Lyamina, E. S. Dvilis, D. T. Valiev, S. A. Stepanov, O. L. Khasanov & A. A. Ditts

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  1. V. D. Paigin
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  2. D. E. Deulina
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  3. A. E. Ilela
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  4. G. V. Lyamina
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  5. E. S. Dvilis
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  6. D. T. Valiev
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  7. S. A. Stepanov
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  8. O. L. Khasanov
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  9. A. A. Ditts
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Correspondence to O. L. Khasanov.

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Translated by O. Zhukova

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Paigin, V.D., Deulina, D.E., Ilela, A.E. et al. Synthesis and Investigation of the Properties of Al2O3–Y2O3 Powders Using Nanospray Drying. rev. and adv. in chem. 12, 270–276 (2022). https://doi.org/10.1134/S2634827623700095

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  • DOI: https://doi.org/10.1134/S2634827623700095

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