Abstract—A study was made of the structure of a VT41 titanium alloy (Ti–Al–Si–Zr–Sn + β stabilizers) subjected to hot upsetting in the (α + β) region, i.e., under conditions simulating the forging process of a disk used for a gas turbine engine (GTE). It reveals the features of the textural state formation of primary and secondary globular grains, as well as the kinetics of their dissolution with increasing annealing temperature. The homogeneity of the billet structure resulting from heat treatment at 995°C increases substantially compared to the deformed state, which is related to the recrystallization of lamellar and small-globular grains and the retention of primary globular grains of the α phase. The sequence of structural changes upon heating is determined in the annealing temperature range from 950 to 1040°C.
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REFERENCES
Medvedev, P.N., Naprienko, S.A., Kashapov, O.S., Shpagin, A.S., and Popov, I.P., The study of the heterogeneity of the structure of a VT41 titanium alloy billet after thermomechanical treatment, Inorg. Mater.: Appl. Res., 2020, vol. 11, pp. 1273–1279. https://doi.org/10.1134/S2075113320060167
Zhang, X.D., Evans, D.J., Baeslack, W.A., and Fraser, H.L., Effect of long term aging on the microstructural stability and mechanical properties of Ti–6Al–2Cr–2Mo–2Sn–2Zr alloy, Mater. Sci. Eng., A, 2003, vol. 344, pp. 300–311.
Anoshkin, N.F., Brun, M.Ya., and Shakhanova, G.V., Requirements to bimodal structure with optimal complex of mechanical properties and regimes of its obtaining, Titan, 1998, no. 1 (10), pp. 35–41.
Lütjering, G. and Williams, J.C., Titanium, Berlin: Springer, 2007, 2nd ed.
Sauer, C. and Lütjering, G., Influence of layers at grain boundaries on mechanical properties of Ti-alloys, Mater. Sci. Eng., A, 2001, vols. 319–321, pp. 393–397.
Es-Souni, M., Creep behaviour and creep microstructures of a high-temperature titanium alloy Ti–5.8Al–4.0Sn–3.5Zr–0.7Nb–0.35Si–0.06C (Timetal 834). Part I: Primary and steady-state creep, Mater. Charact., 2001, vol. 46, pp. 365–379.
Kashapov, O.S., Pavlova, T.V., Kalashnikov, V.S., and Kondrat’ev, A.R., The influence of thermal treatment modes on the structure and properties of test forgings from VT41 alloy with fine-grained structure, Aviats. Mater. Tekhnol., 2017, no. 3 (48), pp. 3–7. https://doi.org/10.18577/2071-9140-2017-0-3-3-7
Russo, P.A. and Yu, K.O., Effect of Ni, Fe, and primary alpha on the creep of alpha-beta processed and annealed Ti–6Al–2Sn–4Zr–2Mo–0.09Si, Proc. 9th World Conf. on “Titanium’99: Science and Technology,” June 7–11, 1999, St. Petersburg: Centr. Res. Inst. Struct. Mater. “Prometey,” 2000, vol. 1, pp. 596–603.
Welk, B.A., Microstructural and property relationships in titanium alloy Ti-5553, MSc. Thesis, Columbus, OH: Ohio State Univ., 2010.
Zeng, W.D. and Zhou, Y.G., The influence of microstructure on dwell sensitive fatigue in Ti–6.5Al–3.5Mo–1.5Zr–0.3Si alloy, Mater. Sci. Eng., A, 2000, vol. 290, pp. 33–38.
Gorbovets, M.A. and Nochovnaya, N.A., Influence of microstructure and phase composition of heat-resisting titanium alloys on the fatigue crack growth rate, Tr. VIAM, 2016, no. 4, art. ID 3. https://doi.org/10.18577/2307-6046-2016-0-4-3-3. http://www.viam-works.ru. Accessed December 3, 2018.
Zakharova, L.V., Influence of chemical composition, thermal treatment and structure on cracking sensitivity of titanium alloys to hot-salt stress corrosion, Tr. VIAM, 2016, no. 9, art. ID 11. https://doi.org/10.18577/2307-6046-2016-0-9-11-11. http://www.viam-works.ru. Accessed December 3, 2018.
Orlov, M.R. and Naprienko, S.A., Destruction of two-phase titanium alloys in sea water, Tr. VIAM, 2017, no. 1, art. ID 10. https://doi.org/10.18577/2307-6046-2017-0-1-10-10. http://www.viam-works.ru. Accessed December 3, 2018.
Kablov, E.N., Kovalev, I.E., Zhemanyuk, P.D., Tkachenko, V.V., Voitenko, S.A., Pirogov, L.A., Banas, F.P., and Kovalev, A.E., Efficiency of surface cold-work hardening of titanium alloys having different phase composition, Proc. 5th Int. Conf. on Computer Methods and Experimental Measurements for Surface Treatment Effects, Computational and Experimental Methods, Seville, 2001, pp. 23–32.
Kablov, E.N., Kashapov, O.S., Pavlova, T.V., and Nochovnaya, N.A., Development of experimental-industrial technology for manufacturing semi-finished products from pseudo-α-titanium alloy VT41, Titan, 2016, no. 2 (52), pp. 33–42.
Kashapov, O.S., Pavlova, T.V., Kalashnikov, V.S., and Zavodov, A.V., Influence of cooling conditions of large industrial forgings from heat-resistant titanium alloy VT41 on the phase composition and mechanical properties, Tsvetn. Met., 2018, no. 2, pp. 76–82. https://doi.org/10.17580/tsm.2018.02.10
Gao, P. et al., Crystallographic orientation evolution during the development of tri-modal microstructure in the hot working of TA15 titanium alloy, J. Alloys C-ompd., 2018, vol. 741, pp. 734–745.
Semiatin, S.L., Seetharaman, V., and Ghosh, A.K., Plastic flow, microstructure evolution, and defect formation during primary hot working of titanium and titanium aluminide alloys with lamellar colony microstructures, Philos. Trans. R. Soc. London, Ser. A, 1999, vol. 357, pp. 1487–1512.
Shell, E.B. and Semiatin, S.L., Effect of initial microstructure on plastic flow and dynamic globularization during hot working of Ti–6Al–4V, Metall. Mater. Trans. A, 1999, vol. 30, pp. 3219–3229.
Seshacharyulu, T. et al., Microstructural mechanisms during hot working of commercial grade Ti–6Al–4V with lamellar starting structure, Mater. Sci. Eng., A, 2002, vol. 325, pp. 112–125.
Yeom, J.-T., Kim, J.H., et al., Characterization of dynamic globularization behavior during hot working of Ti–6Al–4V alloy, Adv. Mater. Res., 2007, vols. 26–28, pp. 1033–1036.
Haisheng, C. et al., Hot deformation behavior and processing map of Ti–6Al–3Nb–2Zr–1Mo titanium alloy, Rare Met. Mater. Eng., 2016, vol. 45, no. 4, pp. 901–906.
Sun, Z.-C., Li, X.S., Wu, H.L., and Yang, H., Morphology evolution and growth mechanism of the secondary Widmanstatten α phase in the TA15 Ti-alloy, Mater. Charact., 2016, vol. 118, pp. 167–174.
Xu, J., Zeng, W., Ma, H., and Zhou, D., Static globularization mechanism of Ti-17 alloy during heat treatment, J. Alloys Compd., 2017, vol. 736, pp. 99–107.
Stefansson, N. and Semiatin, S.L., Mechanism of globularization of Ti–6Al–4V during static heat treatment, Metall. Mater. Trans. A, 2003, vol. 34, pp. 691–698.
Kablov, E.N., Strategic development of the materials and technologies for their recycling until 2030, Aviats. Mater. Tekhnol., 2012, no. S, pp. 7–17.
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Medvedev, P.N., Naprienko, S.A., Kashapov, O.S. et al. Changes in the Structural and Textural States of VT41 Titanium Alloy Resulting from Hot Upsetting and Subsequent Annealing. Inorg. Mater. Appl. Res. 13, 1499–1505 (2022). https://doi.org/10.1134/S2075113322060168
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DOI: https://doi.org/10.1134/S2075113322060168