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A calorimetric study of the process of formation of a supramolecular high-density polyethylene structure in mixtures with different oxides after plastic deformation under high pressure

  • Physicochemical Processes at the Interfaces
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Abstract

Mixtures of ultrahigh-molecular-weight polyethylene with 95 wt % oxides of different elements were subjected to plastic deformation under the pressure of 1 GPa at a high pressure device of the Bridgman anvil type and thermal effects were studied using the DSC technique. Thermograms contained exothermic peaks with a maximum at 50–90°C related to cold crystallization of the polymer. The process of polymer fusion was described by two peaks with the maximums at T 1 = 125–128°C and T 2 = 136–139°C. The low-temperature peak was related to fusion of a structure with high amounts of defects formed on the oxide surface.

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Authors and Affiliations

  1. Semenov Institute of Chemical Physics, Russian Academy of Sciences, 119991, Moscow, Russia

    V. A. Zhorin

  2. A.N. Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences, 119071, Moscow, Russia

    M. R. Kiselev & V. A. Kotenev

Authors
  1. V. A. Zhorin
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  2. M. R. Kiselev
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  3. V. A. Kotenev
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Correspondence to V. A. Zhorin.

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Zhorin, V.A., Kiselev, M.R. & Kotenev, V.A. A calorimetric study of the process of formation of a supramolecular high-density polyethylene structure in mixtures with different oxides after plastic deformation under high pressure. Prot Met Phys Chem Surf 53, 819–825 (2017). https://doi.org/10.1134/S2070205117050276

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  • DOI: https://doi.org/10.1134/S2070205117050276

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