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Extraction of Terpenes of Common Juniper Greenery Under Sub- and Supercritical Conditions

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Abstract

The efficiency of the extraction of the terpene fraction from the greenery of common juniper (Juniperus communis L.) by sub- and supercritical extraction methods is compared with the efficiency of conventional methods. The effect of the extraction parameters on the qualitative composition of the extracts is studied. The components of the obtained extracts are identified by gas chromatography–mass spectrometry. It is determined that the studied extracts are similar in qualitative composition, but differ markedly in the quantitative ratio of groups of components. It is shown that monoterpenes are best extracted with butane under subcritical conditions and by hydrodistillation.

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ACKNOWLEDGMENTS

This study was supported under the 2022–2024 state assignment no. 122011700252-1 “Physicochemical Fundamentals of Selective Methods of Isolation, Characterization, and Application of Biologically Active Complexes of High-Latitude Plant Objects for Solving Problems of Environmental Monitoring and Health Protection” for the Laverov Federal Center for Integrated Arctic Research, Ural Branch, Russian Academy of Sciences, Arkhangelsk, Russia, using the equipment of the Center for Collective Use of Scientific Equipment “Arctika,” Lomonosov Northern (Arctic) Federal University, Arkhangelsk, Russia, and the Center for Collective Use of Scientific Equipment “Critical Technologies of the Russian Federation for Environmental Safety in the Arctic,” Laverov Federal Center for Integrated Arctic Research, Ural Branch, Russian Academy of Sciences, Arkhangelsk, Russia.

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Authors and Affiliations

  1. Laverov Federal Center for Integrated Arctic Research, Ural Branch, Russian Academy of Sciences, 163000, Arkhangelsk, Russia

    A. D. Ivakhnov, N. V. Selivanova, A. A. Krasikova, M. A. Gusakova & K. G. Bogolitsyn

  2. Lomonosov Northern (Arctic) Federal University, 163002, Arkhangelsk, Russia

    A. D. Ivakhnov & K. G. Bogolitsyn

  3. Chemical Faculty, Lomonosov Moscow State University, 119991, Moscow, Russia

    A. N. Stavrianidi

Authors
  1. A. D. Ivakhnov
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  2. N. V. Selivanova
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  3. A. A. Krasikova
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  4. A. N. Stavrianidi
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  5. M. A. Gusakova
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  6. K. G. Bogolitsyn
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Corresponding author

Correspondence to A. A. Krasikova.

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Translated by V. Glyanchenko

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Ivakhnov, A.D., Selivanova, N.V., Krasikova, A.A. et al. Extraction of Terpenes of Common Juniper Greenery Under Sub- and Supercritical Conditions. Russ. J. Phys. Chem. B 16, 1354–1360 (2022). https://doi.org/10.1134/S1990793122080097

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  • DOI: https://doi.org/10.1134/S1990793122080097

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