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Occurrence of Large-Scale Maldistribution of Local Parameters of Mixture Flows across Cross Section of Structured Packing Distillation Column

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Journal of Engineering Thermophysics Aims and scope

Abstract

This paper presents experimental results on occurrence of large-scale maldistribution of parameters of liquid and vapor flows in a regular-packing distillation column. Experiments on separation of mixtures of R114/R21 freons were conducted in a Mellapak 350.Y packing of 0.9 m in diameter. Temperature distributions across column cross sections at different heights were obtained. The experimental studies revealed appearance of large-scale maldistribution of local parameters (temperature and density) across the cross section and height of distillation column when the concentration differential across the column height achieves certain values under conditions of negative stratification of vapor density. An estimative analysis of occurrence of large-scale unevenness under conditions of negative stratification of vapor flow density was done. The experimental data will serve as basis for calculating the efficiency of separation of mixtures in structured packings of column apparatuses to make allowance for the effects of the scale factor associated with large-scale maldistribution of local flow parameters.

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REFERENCES

  1. Bessoua, V., Rouzineau, D., Prévost, M., Abbé, F., Dumont, Ch., Maumus, J-P., and Meyer, M., Performance Characteristics of a New Structured Packing, Chem. Engin. Sci., 2010, vol. 65, no. 16, pp. 4855–4865; DOI:10.1016/j.ces.2010.05.029.

  2. Pavlenko, A.N., Zhukov, V.E., Pecherkin, N.I., Chekhovich, V.Yu., Volodin, O.A., Shilkin, A., and Grossmann, C., Investigation of Flow Parameters and Efficiency of Mixture Separation on a Structured Packing, AIChE, 2014, vol. 60, no. 2, pp. 690–705; DOI:10.1002/aic.14298.

  3. Sun, B., He, L., Liu, B.T., Gu, F., and Liu, C.J., A New Multi-Scale Model Based on CFD and Macroscopic Calculation for Corrugated Structured Packing Column, AIChE, 2013, vol. 59, no. 8, pp. 3119–3130; DOI:10.1002/aic.14082.

  4. Chen, J.B., Liu, C.J., Yuan, X.G., and Yu, G.C., CFD Simulation of Flow and Mass Transfer in Structured Packing Distillation Columns,Chinese J. Chem. Engin., 2009, vol. 17, no. 3, pp. 381–388; DOI:10.1016/S1004-9541(08)60220-7.

  5. Chen, J.B., Liu, C.J., Li, Y.K., Huang, Y., Yuan, X.G., and Yu, G.C., Experimental Investigation of Single-Phase Flow in Structured Packing by LDV, Chinese J. Chem. Engin., 2007, vol. 15, no. 6, pp. 821–827; DOI:10.1016/S1004-9541(08)60009-9.

  6. Egorov, Y., Menter, F., Klöker, M., and Kenig, E.Y., On the Combination of CFD and Rate Based Modelling in the Simulation of Reactive Separation Processes, Chem. Engin. Proc.: Proc. Intens., 2005, vol. 44, no. 6, pp. 631–644; DOI:10.1016/j.cep.2003.10.011.

  7. Larachi, F., Petre, C.F., Iliuta, I., and Grandjean, B., Tailoring the Pressure Drop of Structured Packings through CFD Simulations, Chem. Engin. Proc.: Proc. Intens., 2003, vol. 42, no. 7, pp. 535–541; DOI:10.1016/S0255-2701(02)00073-9.

  8. Petre, C.F., Larachi, F., Iliuta, I., and Grandjean, B., Pressure Drop through Structured Packings: Breakdown into the Contributing Mechanisms by CFD Modeling, Chem. Engin. Sci., 2003, vol. 58, no. 1, pp. 163–177; DOI:10.1016/S0009-2509(02)00473-6.

  9. Szulczewska, B., Zbicinski, I., and Gorak, A., Liquid Flow on Structured Packing: CFD Simulation and Experimental Study,Chem. Engin. Technol., 2003, vol. 26, no. 5, pp. 580–584; DOI:10.1002/ceat.200390089.

  10. Raynal, L., Boyer, C., and Ballaguet, J.P., Liquid Holdup and Pressure Drop Determination in Structured Packing with CFD Simulations, Canadian J. Chem. Engin., 2004, vol. 82, no. 5, pp. 871–879; DOI:10.1002/cjce.5450820502.

  11. Gu, F., Liu, C.J., Yuan, X.G., and Yu, G.C., CFD Simulation of Liquid Film Flow on Inclined Plates, Chem. Engin. Technol., 2004, vol. 27, no. 10, pp. 1099–1104; DOI:10.1002/ceat.200402018.

  12. Fernandes, J., Simoes, P.C., Mota, J.P.B., and Saatdjian, E., Application of CFD in the Study of Supercritical Fluid Extraction with Structured Packing: Dry Pressure Drop Calculations, J. Supercrit. Fluids, 2008, vol. 47, no. 1, pp. 17–24; DOI:10.1016/j.supflu.2008.07.008.

  13. Fernandes, J., Lisboa, F.P., Simoes, P.C., Mota, J.P.B., and Saatdjian, E., Application of CFD in the Study of Supercritical Fluid Extraction with Structured Packing: Wet Pressure Drop Calculations,J. Supercrit. Fluids, 2009, vol. 50, no. 1, pp. 61–68; DOI:10.1016/j.supflu.2009.04.009.

  14. Khosravi Nikou, M.R. and Ehsani, M.R., Turbulence Models Application on CFD Simulation of Hydrodynamics, Heat and Mass Transfer in a Structured Packing, Int. Commun. Heat Mass Transfer, 2008, vol. 35, no. 9, pp. 1211–1219; DOI:10.1016/j.icheatmasstransfer.2008.05.017.

  15. Sivieri, F.M. and Teixeira, E.P., Identification of the Dynamic Model of a Distillation Column, Int. J. Adv. Engin. Res. Sci., 2019, vol. 6, no. 6, pp. 466–470; DOI:10.22161/ijaers.6.6.47.

  16. Pavlenko, A.N., Zhukov, V.E., Pecherkin, N.I., Nazarov, A.D., Slesareva, E.Yu., Li, X., and Sui, H., Efficiency of Mixture Separation in Distillation Columns with Structured Packings under Conditions of Dynamically Controlled Irrigation, J. Eng. Therm., 2019, vol. 28, no. 3, pp. 313–323; DOI:10.1134/S1810232819030020.

  17. Boyadjiev, Chr., Boyadjiev, B., Doichinova, M., and Popova-Krumova, P., Modeling of Column Apparatus Processes, 2nd ed., Springer, 2018, p. 456; DOI:10.1007/978-3-319-89966-4.

  18. Boyadjiev, Chr. and Boyadjiev, B., New Approach to Modeling and Simulation of Chemical and Mass Transfer Processes in Column Apparatuses, Recent Innovat. Chem. Engin. (FormerlyRecent Patents Chem. Engin.), 2019, vol.12, no. 1, pp. 79–95; DOI:10.2174/2405520411666181102161727.

  19. Pavlenko, A.N., Zhukov, V.E., Pecherkin, N.I., Chekhovich, V.Yu., Sunder, S., and Houghton, P., Development of Mixture Composition Maldistribution in a Distillation Column with Structured Packing, Theoretical Found. Chem. Engin., 2010, vol. 44, no. 6, pp. 869–876; DOI: 10.1134/s0040579510060060.

  20. Serov, A.F., Pavlenko, A.N., Pecherkin, N.I., Nazarov, A.D., Krotov, S.V., and Zhukov, V.E., Bubble Flow Rate Meter for the Study of Jet-Droplet Flows in Mass-Exchange Apparatuses, Instruments Exp. Techniq., 1998, vol. 41, no. 5, pp. 727–731.

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Funding

The study was carried out at Kutateladze Institute of Thermophysics SB RAS and financially supported by RFBR (project no. 19-58-18004-Bolgaria_a).

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Correspondence to A. N. Pavlenko.

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Pavlenko, A.N., Zhukov, V.E., Pecherkin, N.I. et al. Occurrence of Large-Scale Maldistribution of Local Parameters of Mixture Flows across Cross Section of Structured Packing Distillation Column. J. Engin. Thermophys. 29, 195–204 (2020). https://doi.org/10.1134/S1810232820020010

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  • DOI: https://doi.org/10.1134/S1810232820020010

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