In our study, SiC foam material has been applied to produce corrugated structured packing in distillation. Three kinds of novel packing with different pore size and corrugation angle have been developed and tested in pilot scale, respectively, to investigate the influence of structural parameters on the performance of SiC foam corrugated structured packing. Hydraulic parameters including pressure drop for dry and wet packing and flooding velocity are determined in an organic glass tower of 600 mm internal diameter, using gas–water. Mass transfer efficiency (HETP) is measured by total reflux experiments in a column with a 310 mm diameter at atmospheric pressure, using a mixture of n-heptane and cyclohexane. The experimental results indicate that SFP-500YD3 with a smaller pore size has higher dry and wet pressure drop, lower flooding velocity and higher mass transfer efficiency compared with SFP-500Y-D5. SFP-500X-D3 with a 30° corrugation angle exhibits lowest pressure drop and highest separation efficiency among all three packings. This study reveals the influence of structural characteristics of SiC foam corrugated structured packing on its performance.
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Dai, C., Xiang, Y., and Lei, Z., Mass Transfer and Hydraulic Performance of CO2 Absorption by Ionic Liquids over Structured Packings, CIESC J., 2015, vol. 66, pp. 2953–2961.
Cong, H., Wang, C., Gao, X., Li, X., Li, H., and Pavlenko, A.N., Pressure Drop Simulation of Structured Corrugation Foam Packing by Computational Fluid Dynamics, J. Eng. Therm., 2016, vol. 25, pp. 301–313.
Olujić, Ž., Kaibel, B., Jansen, H., Rietfort, T., and Zich, E., Fractionation Research Inc. Test Data and Modeling of a High-Performance Structured Packing, Ind. Eng. Chem. Res., 2013, vol. 52, pp. 4888–4894.
Li, Q., Wang, T., Dai, C., and Lei, Z., Hydrodynamics of Novel Structured Packings: An Experimental and Multi-Scale CFD Study, Chem. Eng. Sci., 2016, vol. 143, pp. 23–35.
Jing, W., Hua, W., Zhenzhen, H., and Jinyu, H., Electrodeposited Porous Pb Electrode with Improved Electrocatalytic Performance for the Electroreduction of CO2 to Formic Acid, Front.Chem. Sci. Eng., 2015, vol. 9, pp. 57–63.
Masson, R., Keller, V., and Keller, N., β-SiC Alveolar Foams as a Structured Photocatalytic Support for the Gas Phase Photocatalytic Degradation of Methylethylketone, Appl. Catal., B, 2015, vols. 170/171, pp. 301–311.
Labuschagne, J., Meyer, R., Chonco, Z.H., Botha, J.M., and Moodley, D.J., Application of Water-Tolerant Co/β-SiC Catalysts in Slurry Phase Fischer–Tropsch Synthesis, Catal. Today, 2016, vol. 275, pp. 2–10.
Elamin, M.M., Muraza, O., Malaibari, Z., Ba, H., Nhut, J.-M., and Pham-Huu, C., Microwave Assisted Growth of SAPO-34 on β-SiC Foams for Methanol Dehydration to Dimethyl Ether, Chem. Eng. J., 2015, vol. 274, pp. 113–122.
Sun, M., Chen, C., Chen, L., and Su, B., Hierarchically Porous Materials: Synthesis Strategies and Emerging Applications, Front. Chem. Sci. Eng., 2016, vol. 10, pp. 301–347.
Li, X., Yan, P., Li, H., and Gao, X., Fabrication of Tunable, Stable, and Predictable Superhydrophobic Coatings on Foam CeramicMaterials, Ind. Eng. Chem. Res., 2016, vol. 55, pp. 10095–10103.
Xu, Z., Lu, Y., and Xie, Y., Hydrodynamic and Heat andMass Transfer Performances of Novel Ceramic Foam Packing to Humidification Tower, Appl. Therm. Eng., 2015, vol. 87, pp. 707–713.
Lévêque, J., Rouzineau, D., Prévost, M., and Meyer, M., Hydrodynamic and Mass Transfer Efficiency of Ceramic Foam Packing Applied to Distillation, Chem. Eng. Sci., 2009, vol. 64, pp. 2607–2616.
Lacroix, M., Nguyen, P., Schweich, D., Huu, C.P., Savin-Poncet, S., and Edouard, D., Pressure Drop Measurements and Modeling on SiC Foams, Chem. Eng. Sci., 2007, vol. 62, pp. 3259–3267.
Grosse, J. and Kind, M., Hydrodynamics of Ceramic Sponges in Countercurrent Flow, Ind. Eng. Chem. Res., 2011, vol. 50, pp. 4631–4640.
Pavlenko, A.N., Pecherkin, N.I., Chekhovich, V.Y., Zhukov, V.E., Sunder, S., and Houghton, Experimental Study of the Effect of Maldistribution at the Structured Packing Inlet on the Freon Mixture Separation Efficiency, Theor. Found. Chem. Eng., 2009, vol. 43, pp. 1–11.
Stemmet, C., Bartelds, F., Van der Schaaf, J., Kuster, B., and Schouten, J., Influence of Liquid Viscosity and Surface Tension on the Gas–Liquid Mass Transfer Coefficient for Solid Foam Packings in Co-Current Two-Phase Flow, Chem. Eng. Res. Des., 2008, vol. 86, pp. 1094–1106.
Stemmet, C., Jongmans, J., Van der Schaaf, J., Kuster, B., and Schouten, J., Hydrodynamics of Gas–Liquid Counter-Current Flow in Solid Foam Packings, Chem. Eng. Sci., 2005, vol. 60, pp. 6422–6429.
Chen, T., Lin, Q., Xiong, L., Lü, Q., and Fang, C., Preparation and Characterization of Carbon Foams from Cyanate EsterMixtures, J. Anal. Appl. Pyrol., 2015, vol. 113, pp. 539–544.
Weng, X., Hu, H., Lai, Z., Zhuang, D., and Ding, G., Analysis of Influence of Pore Density on Heat Transfer and Pressure Drop Characteristics ofWet Air inMetal Foams, CIESC J., 2016, vol. 67, pp. 2218–2223.
Pavlenko, A., Zhukov, V., Pecherkin, N., Chekhovich, V., Volodin, O., Shilkin, A., et al., Investigation of Flow Parameters and Efficiency of Mixture Separation on a Structured Packing, AIChE J., 2014, vol. 60, pp. 690–705.
Li, H., Wang, F., Wang, C., Gao, X., and Li, X., Liquid Flow Behavior Study in SiC Foam Corrugated Sheet Using a Novel Ultraviolet Fluorescence Technique Coupled with CFD Simulation, Chem. Eng. Sci., 2015, vol. 123, pp. 341–349.
Li, X., Liu, Q., Li, H., and Gao, X., Experimental Study on Liquid Flow Behavior in the Holes of SiC Structured Corrugated Sheets, J. Taiwan Inst. Chem. Eng., 2016, vol. 64, pp. 39–46.
Liu, Q., Li, H., Gao, X., and Li, X., Liquid Flow Characteristics of Structured Corrugation SiC-Foam Packing Sheets, CIESC J., 2016, vol. 67, pp. 3340–3346.
Li, X., Gao, G., Zhang, L., Sui, H., Li, H., Gao, X., et al., Multiscale Simulation and Experimental Study of Novel SiC Structured Packings, Ind. Eng. Chem. Res., 2011, vol. 51, pp. 915–924.
Zhang, J., Tian, C., Yang, Z., Cao, X., Liu, Q., Li, X. et al., A Preparation Methods and Application of SiC Ceramic Foam Structured Corrugated Packing, Institute ofMetal Research, 2010.
Qiao, Y., Gao, X., Li, H., and Li, X., Life Cycle Cost Evaluation of Structured Corrugation SiC-Foam Packing, CIESC J., 2016, vol. 67, pp. 3459–3467.
Yao, Y., Pavlenko, A.N., and Volodin, O.A., Effects of Layers and Holes on Performance of Wire Mesh Packing, J. Eng. Therm., 2015, vol. 24, pp. 222–236.
Amini, Y., Karimi-Sabet, J., and Esfahany, M.N., Characterization of New Wire Gauze High-Capacity Structured Packing with Varied Inclination Angle, Chem. Eng. Technol., 2017, vol. 40, pp. 581–587.
Li, H., Yao, Y., Wang, F., Gao, X., and Li, X., Effect of Liquid Flow Behavior on Performance of Corrugated Structured Packing, CIESC J., 2014, vol. 65, pp. 4760–4766.
Olujić, Ž., Seibert, A.F., and Fair, J.R., Influence of Corrugation Geometry on the Performance of Structured Packings: An Experimental Study, Chem. Eng. Prog., 1991, vol. 39, pp. 335–342.
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Li, X., Shi, Q., Li, H. et al. Experimental characterization of novel SiC foam corrugated structured packing with varied pore size and corrugation angle. J. Engin. Thermophys. 26, 452–465 (2017). https://doi.org/10.1134/S1810232817040026