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Synthesis and Characterization of Ethylene Glycol-Polydimethylsiloxane-Polybutyl Methacrylate Copolymer

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Abstract—

In this article, the octamethylcyclotetrasiloxane is introduced into ethylene glycol. The reaction is terminated using acrylic acid to obtain a linear polydimethylsiloxane intermediate comprising double bonds at the ends. The targeted copolymer is prepared by copolymerizing polydimethylsiloxane intermediate and butyl methacrylate. Additionally, blended-porous film is prepared by adding the copolymer to the cyclodextrin copolymer. The results reveal that the thermal stability of the copolymer increases with the increase of the polydimethylsiloxane content. The ethanol solution of the copolymer of a certain formulation has temperature sensitivity. The contact angle hysteresis of cyclodextrin copolymer is larger on the inclined surface at five degrees from the horizontal, but the blended-porous films all have low contact angle hysteresis, and the minimum contact angle hysteresis decreased to 2°. The main reason for the observed difference is that the presence of the copolymer makes the surface morphology of the film changed greatly. The blended-porous films have a waterproof and easy-to-slide surface.

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Funding

The authors are grateful for the sponsorship of the Support Program (Industrial) of Changzhou Science and Technology (CE20200014), the Top-notch Academic Programs Project of Jiangsu Higher Education Institutions (TAPP), the Postgraduate Research & Practice Innovation Program of Jiangsu Province (SJCX21_1181), the Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD), Jiangsu Chenguang Paint Co., Ltd, Changzhou, Jiangsu, and Shenzhen Basic Research Project (JCYJ20170818114324998).

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Authors and Affiliations

  1. National Experimental Demonstration Center for Materials Science and Engineering Changzhou University, 213164, Changzhou, China

    Juan Chen, Xiaomei Zhang, Yuying Chen, Xing Lin, Yan Jiang & Hongwen Zhang

  2. School of Chemistry, Shenzhen Vocational and Technical College, 518005, Shenzhen, China

    Hongbo Liu

  3. Jiangsu Chenguang Paint Co., Ltd., 213154, Changzhou, Jiangsu, China

    Yan Jiang

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  1. Juan Chen
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  2. Xiaomei Zhang
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  3. Yuying Chen
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  5. Yan Jiang
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  6. Hongwen Zhang
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  7. Hongbo Liu
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Correspondence to Yan Jiang.

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Juan Chen, Zhang, X., Chen, Y. et al. Synthesis and Characterization of Ethylene Glycol-Polydimethylsiloxane-Polybutyl Methacrylate Copolymer. Polym. Sci. Ser. B 64, 429–444 (2022). https://doi.org/10.1134/S1560090422700142

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  • DOI: https://doi.org/10.1134/S1560090422700142

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