Abstract
The effect of technological parameters on the morphological and sorption-structural characteristics of mesoporous materials is described. Recommendations on the production of such materials with narrow and bimodal pore size distribution and the maximum possible specific surface area on the example of the MCM-41 template synthesis are provided.
Similar content being viewed by others
REFERENCES
Tret’yakov, Yu.D., Major directions of basic and dedicated basic research in the area of nanomaterials, Al’tern. Ekol. Energet., 2009, no. 6, pp. 39–67.
Karpov, S.I., Roessner, F., Selemenev, V.F., Gul’bin, S.S., Belanova, N.A., Borodina, E.V., Korabel’nikova, E.O., Krizhanovskaya, O.O., and Nedosekina, I.V., Prospects of synthesis and applications of high ordered mesoporous materials as a sorbents for chromatographic analysis, separation and preconcentration of physiologically active substances (review), Sorbtsion. Khromatogr. Protsessy, 2013, vol. 13, no. 2, pp. 125–140.
Wang, X., Nanocomposites: Synthesis, characterization and applications. State key laboratory of pulp and paper engineering school of light industry and food, PhD Thesis, Guangzhou, China: South China Univ. of Technol., 2013.
Lysenko, S.V., Kryukov, I.O., Sarkisov, O.A., Abikenova, A.B., Baranova, S.V., Ostroumova, V.A., Kardashev, S.V., Kovaleva, N.F., and Karakhanov, E.A., Properties of mesoporous aluminosilicates, prepared with non-ionic surfactants, Mosc. Univ. Chem. Bull., 2011, vol. 66, no. 2, pp. 116–120.
Zherebtsov, D.A., Synthesis of nanomaterials using surfactants, Vestn. YuurGU, Ser. Metallurg., 2019, vol. 19, no. 3, pp. 66–96.
Demirbas, A., Biodiesel a Realistic Fuel Alternative for Diesel Engines, London: Springer, 2008.
Neizvestnaya, S.V., Preparation and application of mesophase mesoporous materials in the processes of obtaining biodiesel fuel using microwave radiation, in Sbornik Nauchnykh statei molodykh uchenykh, aspirantov i studentov: Problemy tekhnogennoi bezopasnosti i ustoichivogo razvitiya (Problems of Technogenic Safety and Sustainable Development, Collection of Scientific Articles of Young Scientists, Graduate Students and Students), 2012, no. 3, pp. 215–218.
Neizvestnaya, S.V., Planning an experiment to study the synthesis of block products based on nanoperiodic silicate and aluminosilicate materials, Vopr. Sovrem. Nauki Prakt., Univ. im. V. I. Vernadskogo, 2011, no. 2 (33), pp. 401–406.
Problemy analiticheskoi khimii. Tom 20. Nanoob’’ekty i nanotekhnologii v khimicheskom analize (Problems of Analytical Chemistry, Vol. 20: Nanoobjects and Nanotechnology in Chemical Analysis), Shtykov, S.N., Ed., Moscow: Nauka, 2015.
Mel’gunova, E.A., Synthesis of mesoporous materials using surfactants Pluronic P123 and study of their texture, Extended Abstract of Cand. Sci. (Chem.) Dissertation, Novosibirsk, 2010.
Brinker, C.J. and Scherer, G.W., Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing, San Diego: Elsevier Science, 1989.
Schmidt-Winkel, P., Lukens, W.W., and Yang, P., Jr., Margolese, D.I., Lettow, J.S., Ying, J.Y., and Stucky, G.D., Microemulsion templating of siliceous mesostructured cellular foams with well-defined ultralarge mesopores, Chem. Mater., 2000, no. 12, pp. 686–696.
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
The authors declare to have no conflict of interest.
Additional information
Translated by D. Marinin
Rights and permissions
About this article
Cite this article
Neizvestnaya, S.V. Effect of Parameters of Synthesis of Mesoporous Materials on the Set of Their Sorption–Texture Properties. Glass Phys Chem 46, 635–639 (2020). https://doi.org/10.1134/S1087659620060176
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1087659620060176