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1,4-Dithiane-2,5-diol as an Efficient Synthon for the Synthesis of Functionalized 1,3,4-Benzothiadiazepine Derivatives

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Abstract

The reaction of 1,4-dithiane-2,5-diol with 2-sulfanylbenzohydrazide afforded 55% of previously unknown 2-(sulfanylmethyl)-1,3,4-benzothiadiazepin-5(2H)-one whose structure was confirmed by 1H and 13C NMR spectra.

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Funding

This work was supported by ongoing institutional funding. No additional grants to carry out or direct this particular research were obtained.

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Authors and Affiliations

  1. Institute of Macromolecular Compounds, Russian Academy of Sciences, 199004, St. Petersburg, Russia

    A. Yu. Ershov & A. A. Martynenkov

  2. State Research Testing Institute of Military Medicine, Ministry of Defense of the Russian Federation, 195043, St. Petersburg, Russia

    I. V. Lagoda & A. A. Batyrenko

Authors
  1. A. Yu. Ershov
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  2. I. V. Lagoda
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  3. A. A. Batyrenko
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  4. A. A. Martynenkov
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Correspondence to A. A. Martynenkov.

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Ershov, A.Y., Lagoda, I.V., Batyrenko, A.A. et al. 1,4-Dithiane-2,5-diol as an Efficient Synthon for the Synthesis of Functionalized 1,3,4-Benzothiadiazepine Derivatives. Russ J Org Chem 59, 2239–2240 (2023). https://doi.org/10.1134/S1070428023120242

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  • DOI: https://doi.org/10.1134/S1070428023120242

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