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Reaction of Methyl 1-Bromocyclohexanecarboxylate with Zinc and 3-Aryl-1-(2-hydroxyphenyl)prop-2-en-1-ones

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Abstract

The reaction of 3-aryl-1-(2-hydroxyphenyl)prop-2-en-1-ones with methyl 1-bromocyclohexanecarboxylate and zinc resulted in the isolation, after hydrolysis of the reaction mixture, of spirodihydropyran-2-ones containing a 1-(2-hydrohybenzoyl)cyclohexyl substituent in the 6-position. The structure of the products was confirmed X-ray diffraction analysis.

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Funding

The work was financially supported by the Russian Foundation for Basic Research (project no. 18-33-00509) and the Government of the Perm Region.

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Authors and Affiliations

  1. Perm State National Research University, 614990, Perm, Russia

    E. A. Nikiforova, D. V. Baibarodskikh, M. V. Dmitriev, D. P. Zverev & N. F. Kirillov

Authors
  1. E. A. Nikiforova
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  2. D. V. Baibarodskikh
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  3. M. V. Dmitriev
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  4. D. P. Zverev
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  5. N. F. Kirillov
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Correspondence to E. A. Nikiforova.

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Nikiforova, E.A., Baibarodskikh, D.V., Dmitriev, M.V. et al. Reaction of Methyl 1-Bromocyclohexanecarboxylate with Zinc and 3-Aryl-1-(2-hydroxyphenyl)prop-2-en-1-ones. Russ J Org Chem 56, 2032–2035 (2020). https://doi.org/10.1134/S1070428020110196

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  • DOI: https://doi.org/10.1134/S1070428020110196

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