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One-Pot Synthesis of 2-Ylidene-1,3-dithiolanes

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Abstract

A one-pot synthesis of 2-ylidene-1,3-dithiolanes, involving the reaction of carbon disulfide with methylene-active compounds in the presence of sodium ethylate followed by adding 1,2-dichloralkanes to the reaction mixture, is developed.

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References

  1. Olk, R.-M., Olk, B., Dietzsch, W., Kirmse, R., and Hoyer, E., Coord. Chem. Rev., 1992, vol.117, p.99. doi https://doi.org/10.1016/0010-8545(92)80021-I

    Article  CAS  Google Scholar 

  2. Pullen, A.E. and Olk, R.-M., Coord. Chem. Rev., 1999, vol.188, p.211. doi https://doi.org/10.1016/S0010-8545(99)00031-4

    Article  CAS  Google Scholar 

  3. Stiefel, E.I. Dithiolene Chemistry: Synthesis, Properties, and Applications, vol. 52, New-York: J. Wiley & Sons Inc., 2004.

  4. Hanaki, N., Motoki, M., and Yawata, T., WO Patent Appl. WO 2009022736, 2009.

  5. Suzuki, H. and Yamada, S., US Patent Appl. no. 2009202921, 2009.

  6. Hanaki, N., Yawata, T., and Mikoshiba, H., US Patent Appl. no 20100025642, 2010.

  7. Hanaki, N. and Yawata, T., US Patent Appl. no. 20100130638, 2010.

  8. Lipin, K.V., Ershov, O.V., Belikov, M.Y., and Fedoseev, S.V., Russ. J. Org. Chem., 2017, vol.53, p.147. doi https://doi.org/10.1134/S1070428017010304

    Article  CAS  Google Scholar 

  9. Gompper, R. and Kutter, E., Chem. Ber., 1965, vol.98, p.1365. doi https://doi.org/10.1002/cber.19650980908

    Article  CAS  Google Scholar 

  10. Didier, V. and Abdelkrim, B.A., Synthesis, 1991, vol.4, p.301. doi https://doi.org/10.1055/s-1991-26449

    Google Scholar 

  11. Jensen, K.A. and Henriksen, L., Acta. Chem. Scand., 1968, vol.22, p.1107. doi https://doi.org/10.3891/acta.chem.scand.22-1107

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Ul’yanov Chuvash State University, Moskovskii pr. 15, Cheboksary, Chuvashia, 428015, Russia

    K. V. Lipin, O. V. Ershov, M. Yu. Belikov & S. V. Fedossev

Authors
  1. K. V. Lipin
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  2. O. V. Ershov
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  3. M. Yu. Belikov
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  4. S. V. Fedossev
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Corresponding author

Correspondence to K. V. Lipin.

Additional information

Russian Text © K.V. Lipin, O.V. Ershov, M.Yu. Belikov, S.V. Fedossev, 2019, published in Zhurnal Organicheskoi Khimii, 2019, Vol. 55, No. 2, pp. 314–316.

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Lipin, K.V., Ershov, O.V., Belikov, M.Y. et al. One-Pot Synthesis of 2-Ylidene-1,3-dithiolanes. Russ J Org Chem 55, 276–278 (2019). https://doi.org/10.1134/S1070428019020246

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  • DOI: https://doi.org/10.1134/S1070428019020246

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