Abstract
The reactions of 5-(arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with arenecarbaldehyde phenylhydrazones in the presence of sodium N-chlorobenzenesulfonamide give 2,3,7,9-tetraasaspiro-[4.5]dec-1-ene-6,8,10-triones in yields of 30–45%.
References
Baranski, A. and Kelarev, V.I., Chem. Heterocycl. Comp., 1990, vol.26, p.371. doi https://doi.org/10.1007/BF00497204
Nosachev, S.B., Candidate Sci. (Chem.) Dissertation, Astrakhan, 2011.
Shchurova, N.A. and Tyrkov, A.G., Zh. Org. Khim., 2006, vol.42, p.1592.
Velikorodov, A.V., Russ. J. Org. Chem., 2004, vol.40, p.1490. doi https://doi.org/10.1007/S1117800500478
Rai Lokanatha, K.M. and Hassner, A., Synth. Commun., 1989, vol.19, p.2799. doi https://doi.org/10.1080/00397918908052667
Gladstone, W.A.F., Aylward, J.B., and Norman, R.O.C., J. Chem. Soc. C, 1969, p.2587. doi https://doi.org/10.1039/J39690002587
Tyrkov, A.G., Nosachev, S.B., and Vladimirova, T.S., Russ. J. Org. Chem., 2016, vol.52, p.762. doi https://doi.org/10.1134/S1070428016050274
Structure Determination of Organic Compounds: Tables of Spectral Data, Pretsch, E., Bühlmann, P., and Affolter, C., Eds., Berlin: Springer, 2000, 3rd ed. Translated under the title Opredelenie stroeniya organicheskikh soedinenii. Tablitsy spektral’nykh dannykh, Moscow: Mir, 2006
Granik, V.G., Osnovy meditsinskoi khimii (Fundamentals of Medical Chemistry), Moscow: Vuzovskaya khiga, 2001.
Kirkhner, Yu., Tonkosloinaya khromatografiya (Thin Layer Chromatography), Moscow: Mir, 1981, vol. 1.
Yurtaeva, E.A. and Tyrkov, A.G., Russ. J. Org. Chem., 2016, vol.52, p.289. doi https://doi.org/10.1134/S1070428016020214
Metody polucheniya khimicheskikh reaktivov i preparatov (Methods of Obtaining Chemical Reagents and Preparations), Moscow: IREA, 1964, vol. 8.
Author information
Authors and Affiliations
Corresponding authors
Additional information
Russian Text © A.G. Tyrkov, E.A. Yurtaeva, O.B. Rsaeva, 2019, published in Zhurnal Organicheskoi Khimii, 2019, Vol. 55, No. 2, pp. 307–310.
Rights and permissions
About this article
Cite this article
Tyrkov, A.G., Yurtaeva, E.A. & Rsaeva, O.B. Reaction 5-(Arylmethylidene)-2,4,6-pyrimidine-2,4,6(1H,3H,5H)-triones with Arenecarbaldehyde Phenylhydrazones in the Presence of Sodium N-Chlorobenzenesulfonamide. Russ J Org Chem 55, 269–272 (2019). https://doi.org/10.1134/S1070428019020222
Received:
Revised:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1070428019020222