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First example of one-pot assembly of tetrasubstituted thiophene with amino- and ester functions from methoxyallene, methyl isothiocyanate, and methyl 2-bromoacetate

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Abstract

The previously unavailable methyl 4-methoxy-3-methyl-5-(methylamino)thiophene-2-carboxylate was obtained by the one-pot procedure from a lithiated methoxyallene, methyl isothiocyanate, and methyl 2-bromoacetate.

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References

  1. Nedolya, N.A., Brandsma, L., Tarasova, O.A., Verkruijsse, H.D., and Trofimov, B.A., Tetrahedron Lett., 1998, vol. 39, p. 2409.

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Authors and Affiliations

  1. Favorskii Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences, ul. Favorskogo 1, Irkutsk, 664033, Russia

    N. A. Nedolya, O. A. Tarasova, A. I. Albanov & B. A. Trofimov

Authors
  1. N. A. Nedolya
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  2. O. A. Tarasova
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  3. A. I. Albanov
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  4. B. A. Trofimov
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Corresponding author

Correspondence to N. A. Nedolya.

Additional information

Original Russian Text © N.A. Nedolya, O.A. Tarasova, A.I. Albanov, B.A. Trofimov, 2017, published in Zhurnal Organicheskoi Khimii, 2017, Vol. 53, No. 8, pp. 1255–1256.

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Nedolya, N.A., Tarasova, O.A., Albanov, A.I. et al. First example of one-pot assembly of tetrasubstituted thiophene with amino- and ester functions from methoxyallene, methyl isothiocyanate, and methyl 2-bromoacetate. Russ J Org Chem 53, 1272–1274 (2017). https://doi.org/10.1134/S1070428017080206

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  • DOI: https://doi.org/10.1134/S1070428017080206

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