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Investigation of reaction between 2-methylimidazole and 1,3-bis(iodomethyl)-1,1,3,3-tetramethyldisiloxane by the method NALDI TOF/TOF

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Abstract

By the method of nanostructure-assisted laser desorption/ionization (NALDI) analysis was performed of solid and liquid fractions of reaction products formed from 2-methylimidazole and 1,3-bis- (iodomethyl)-1,1,3,3-tetramethyldisiloxane. Basing on the data post-source decay of iodides major and minor products of reaction were identified that were registered as ions [M–I]+ and [M–I3]+.

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Authors and Affiliations

  1. Favorskii Irkutsk Institute of Chemistry, Siberian Branch, Russian Academy of Sciences, ul. Favorskogo 1, Irkutsk, 664033, Russia

    L. V. Klyba, E. R. Sanzheeva, L. G. Shagun & L. V. Zhilitskaya

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  1. L. V. Klyba
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  2. E. R. Sanzheeva
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  3. L. G. Shagun
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  4. L. V. Zhilitskaya
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Correspondence to L. V. Zhilitskaya.

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Original Russian Text © L.V. Klyba, E.R. Sanzheeva, L.G. Shagun, L.V. Zhilitskaya, 2017, published in Zhurnal Organicheskoi Khimii, 2017, Vol. 53, No. 8, pp. 1217–1222.

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Klyba, L.V., Sanzheeva, E.R., Shagun, L.G. et al. Investigation of reaction between 2-methylimidazole and 1,3-bis(iodomethyl)-1,1,3,3-tetramethyldisiloxane by the method NALDI TOF/TOF. Russ J Org Chem 53, 1233–1238 (2017). https://doi.org/10.1134/S1070428017080127

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  • DOI: https://doi.org/10.1134/S1070428017080127

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