Skip to main content
Log in

Synthesis of some 2-ylidene-1,3-dithiolanes

  • Short Communications
  • Published:
Russian Journal of Organic Chemistry Aims and scope Submit manuscript

Abstract

Convenient procedures have been developed for the synthesis of 2-(1,3-dithiolan-2-ylidene)- malononitriles and 2-cyano-2-(1,3-dithiolan-2-ylidene)acetamides from disodium alk-1-ene-1,1-dithiolates and 1,2-dichloroalkanes, as well as from malononitrile or cyanoacetamide in a one-pot mode.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

References

  1. Olk, R.-M., Olk, B., Dietzsch, W., Kirmse, R., and Hoyer, E., Coord. Chem. Rev., 1992, vol. 117, p. 99.

    Article  CAS  Google Scholar 

  2. Pullen, A.E. and Olk, R.-M., Coord. Chem. Rev., 1999, vol. 188, p. 211.

    Article  CAS  Google Scholar 

  3. Dithiolene Chemistry: Synthesis, Properties, and Applications, Stiefel, E.I., Ed., New York: Wiley, 2004.

  4. Hanaki, N., Motoki, M., and Yawata, T., WO Patent no. 2009/022736.

    Google Scholar 

  5. Suzuki, H. and Yamada, S., US Patent no. 2009/202921.

    Google Scholar 

  6. Hanaki, N., Yawata, T., and Mikoshiba, H., US Patent no. 2010/0025642.

    Google Scholar 

  7. Hanaki, N. and Yawata, T., US Patent no. 2010/0130638.

    Google Scholar 

  8. Gompper, R. and Töpfl, W., Chem. Ber., 1962, vol. 95, p. 2861.

    Article  CAS  Google Scholar 

  9. Jensen, K.A. and Henriksen, L., Acta. Chem. Scand., 1968, vol. 22, p. 1107.

    Article  CAS  Google Scholar 

  10. Didier, V. and Abdelkrim, B.A., Synthesis, 1991, no. 4, p. 301.

    Google Scholar 

  11. Söderbäck, E., Acta. Chem. Scand., 1963, vol. 17, p. 362.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to K. V. Lipin.

Additional information

Original Russian Text © K.V. Lipin, O.V. Ershov, M.Yu. Belikov, S.V. Fedoseev, 2017, published in Zhurnal Organicheskoi Khimii, 2017, Vol. 53, No. 1, pp. 148–150.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lipin, K.V., Ershov, O.V., Belikov, M.Y. et al. Synthesis of some 2-ylidene-1,3-dithiolanes. Russ J Org Chem 53, 147–149 (2017). https://doi.org/10.1134/S1070428017010304

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1070428017010304

Navigation