Advertisement

Russian Journal of Organic Chemistry

, Volume 53, Issue 1, pp 147–149 | Cite as

Synthesis of some 2-ylidene-1,3-dithiolanes

  • K. V. LipinEmail author
  • O. V. Ershov
  • M. Yu. Belikov
  • S. V. Fedoseev
Short Communications
  • 47 Downloads

Abstract

Convenient procedures have been developed for the synthesis of 2-(1,3-dithiolan-2-ylidene)- malononitriles and 2-cyano-2-(1,3-dithiolan-2-ylidene)acetamides from disodium alk-1-ene-1,1-dithiolates and 1,2-dichloroalkanes, as well as from malononitrile or cyanoacetamide in a one-pot mode.

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. 1.
    Olk, R.-M., Olk, B., Dietzsch, W., Kirmse, R., and Hoyer, E., Coord. Chem. Rev., 1992, vol. 117, p. 99.CrossRefGoogle Scholar
  2. 2.
    Pullen, A.E. and Olk, R.-M., Coord. Chem. Rev., 1999, vol. 188, p. 211.CrossRefGoogle Scholar
  3. 3.
    Dithiolene Chemistry: Synthesis, Properties, and Applications, Stiefel, E.I., Ed., New York: Wiley, 2004.Google Scholar
  4. 4.
    Hanaki, N., Motoki, M., and Yawata, T., WO Patent no. 2009/022736.Google Scholar
  5. 5.
    Suzuki, H. and Yamada, S., US Patent no. 2009/202921.Google Scholar
  6. 6.
    Hanaki, N., Yawata, T., and Mikoshiba, H., US Patent no. 2010/0025642.Google Scholar
  7. 7.
    Hanaki, N. and Yawata, T., US Patent no. 2010/0130638.Google Scholar
  8. 8.
    Gompper, R. and Töpfl, W., Chem. Ber., 1962, vol. 95, p. 2861.CrossRefGoogle Scholar
  9. 9.
    Jensen, K.A. and Henriksen, L., Acta. Chem. Scand., 1968, vol. 22, p. 1107.CrossRefGoogle Scholar
  10. 10.
    Didier, V. and Abdelkrim, B.A., Synthesis, 1991, no. 4, p. 301.Google Scholar
  11. 11.
    Söderbäck, E., Acta. Chem. Scand., 1963, vol. 17, p. 362.CrossRefGoogle Scholar

Copyright information

© Pleiades Publishing, Ltd. 2017

Authors and Affiliations

  • K. V. Lipin
    • 1
    Email author
  • O. V. Ershov
    • 1
  • M. Yu. Belikov
    • 1
  • S. V. Fedoseev
    • 1
  1. 1.I.N. Ul’yanov Chuvash State UniversityCheboksaryRussia

Personalised recommendations