Abstract
An efficient procedure has been developed for the synthesis of N-cycloalkyl-1,5,3-dithiazepanes by recyclization of 1-oxa-3,6-dithiacycloheptane with cycloalkylamines in the presence of SmCl3 · 6 H2O as catalyst.
Similar content being viewed by others
References
Ito, K. and Sekiya, M., Chem. Pharm. Bull., 1979, vol. 27, p. 1691.
Khabibullina, G.R., Akhmetova, V.R., Abdullin, M.F., Tyumkina, T.V., Khalilov, L.M., Ibragimov, A.G., and Dzhemilev, U.M., Tetrahedron, 2014, vol. 70, p. 3502.
Rakhimova, E.B., Vasil’yeva, I.V., Khalilov, L.M., Ibragimov, A.G., and Dzhemilev, U.M., Chem. Heterocycl. Compd., 2012, vol. 48, no. 7, p. 1050.
Rakhimova, E.B., Meshcheryakova, E.S., Khalilov, L.M., Ibragimov, A.G., and Dzhemilev, U.M., Russ. J. Org. Chem., 2014, vol. 50, p. 1613.
Rakhimova, E.B., Efremova, E.A., Bushmarinov, I.S., Goloveshkin, A.S., Khalilov, L.M., Ibragimov, A.G., and Dzhemilev, U.M., Tetrahedron Lett., 2012, vol. 53, p. 4225.
Rakhimova, E.B., Ismagilov, R.A., Meshcheryakova, E.S., Zainullin, R.A., Khalilov, L.M., Ibragimov, A.G., and Dzhemilev, U.M., Chem. Heterocycl. Compd., 2014, vol. 5, p. 720.
Ameta, K.L., Pawar, R.P., and Domb, A.J., Bioactive Heterocycles: Synthesis and Biological Evaluation, Hauppauge, NY: Nova Science, 2012.
Akhmetova, V.R. and Rakhimova, E.B., Russ. J. Org. Chem., 2014, vol. 50, p. 1711.
Voronin, S.P., Gubina, T.I., Trushin, S.A., Markushina, I.A., and Kharchenko, V.G., Chem. Heterocyclic. Compd., 1989, vol. 11, p. 1216.
Kukushkin, Yu.N., Reaktsionnaya sposobnost’ koordinatsionnykh soedinenii (Reactivity of Coordination Compounds), Leningrad: Khimiya, 1987, p. 288.
Author information
Authors and Affiliations
Corresponding author
Additional information
Original Russian Text © E.B. Rakhimova, R.A. Ismagilov, L.M. Khalilov, R.A. Zainullin, A.G. Ibragimov, U.M. Dzhemilev, 2015, published in Zhurnal Organicheskoi Khimii, 2015, Vol. 51, No. 7, pp. 971–976.
Rights and permissions
About this article
Cite this article
Rakhimova, E.B., Ismagilov, R.A., Khalilov, L.M. et al. Efficient catalytic synthesis of N-cycloalkyl-1,5,3-dithiazepanes. Russ J Org Chem 51, 951–956 (2015). https://doi.org/10.1134/S1070428015070118
Received:
Published:
Issue Date:
DOI: https://doi.org/10.1134/S1070428015070118