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Synthesis of 3-hetaryl-1,5,3-dithiazepanes and 3-hetaryl-1,5,3-dithiazocanes in the presence of catalysts based on transition metals

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Abstract

Efficient procedure was developed for 3-hetaryl-1,5,3-dithiazepanes and 3-hetaryl-1,5,3-dithiazocanes preparation from hetarylamines, N,N,N′,N′-tetramethylmethanediamine, and α,ω-alkanedithiols (ethane-1,2-dithiol, propane-1,3-dithiol), and also by the reaction of the latter with N,N-bis(methoxymethyl)hetarylamines in the presence of catalytic quantities of transition metals salts.

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Authors and Affiliations

  1. Institute of Petrochemistry and Catalysis, Russian Academy of Sciences, Ufa, 450075, Russia

    N. N. Makhmudiyarova, K. I. Prokof’ev, L. V. Mudarisova, A. G. Ibragimov & U. M. Dzhemilev

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  1. N. N. Makhmudiyarova
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  2. K. I. Prokof’ev
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  3. L. V. Mudarisova
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  4. A. G. Ibragimov
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  5. U. M. Dzhemilev
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Correspondence to N. N. Makhmudiyarova.

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Original English Text © N.N. Makhmudiyarova, K.I. Prokof’ev, L.V. Mudarisova, A.G. Ibragimov, U.M. Dzhemilev, 2013, published in Zhurnal Organicheskoi Khimii, 2013, Vol. 49, No. 5, pp. 677–681.

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Makhmudiyarova, N.N., Prokof’ev, K.I., Mudarisova, L.V. et al. Synthesis of 3-hetaryl-1,5,3-dithiazepanes and 3-hetaryl-1,5,3-dithiazocanes in the presence of catalysts based on transition metals. Russ J Org Chem 49, 658–662 (2013). https://doi.org/10.1134/S1070428013050035

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  • DOI: https://doi.org/10.1134/S1070428013050035

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