Abstract
Efficient preparation method was developed for N-aryl(benzyl, alkyl)-1,5,3-dithiazocan-3-amines consisting in the transamination of 3-tert-butyl-1,5,3-dithiazocane with aryl(benzyl)hydrazines, and also in the reaction of N 1,N 1,N 7,N 7-tetramethyl-2,6-dithiaheptane-1,7-diamine with aryl(benzyl, alkyl)hydrazines in the presence of catalytic amounts of Ti and Cu compounds.
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Original English Text © N.N. Makhmudiyarova, K.I. Prokof’ev, L.V. Mudarisova, A.G. Ibragimov, U.M. Dzhemilev, 2013, published in Zhurnal Organicheskoi Khimii, 2013, Vol. 49, No. 5, pp. 674–676.
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Makhmudiyarova, N.N., Prokof’ev, K.I., Mudarisova, L.V. et al. Hydrazines in the synthesis of N-substituted 1,5,3-dithiazocan-3-amines catalyzed by Ti and Cu compounds. Russ J Org Chem 49, 655–657 (2013). https://doi.org/10.1134/S1070428013050023
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DOI: https://doi.org/10.1134/S1070428013050023