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Synthesis of 2-aminomethoxy-1-benzylsulfanylpentanes

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Abstract

Mannich condensation of 1-benzylsulfanylpentane with equimolar amounts of formaldehyde and secondary amine gave in 3–4 h at 45–50°C the corresponding 2-aminomethoxy-1-benzylsulfanylpentanes in 72–76% yield.

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References

  1. Mashkovskii, M.D., Lekarstvennye sredstva (Drugs), Moscow: Novaya Volna, 2006; Kharkevich, D.A., Farmakologiya (Pharmacology), Moscow: Geotar Meditsina, 2005; Beletskaya, I.P. and Cheprakov, A.V., Coord. Chem. Rev., 2004, vol. 248, p. 2337; Beletskaya, I.P. and Ananikov, V.P., Eur. J. Org. Chem., 2007, p. 3431; Fetterly, B.M., Janna, N.K., and Verkade, J.G., Tetrahedron, 2006, vol. 62, p. 440.

    Google Scholar 

  2. Kuliev, A.M., Khimiya i tekhnologiya prisadok k maslam i toplivam (Chemistry and Technology of Oil and Fuel Additives), Moscow: Khimiya, 1972; Allakhverdiev, M.A., Akperov, N.A., Mustafaev, K.N., and Farzaliev, V.M., Neftekhimiya, 2001, vol. 41, p. 325; Allakhverdiev, M.A. Mustafaev, K.N., and Farzaliev, V.M., Russ. J. Org. Chem., 2002, vol. 38, p. 1620.

    Google Scholar 

  3. Voronkov, M.G. and Deryagina, A.V., Usp. Khim., 2000, vol. 69, p. 50; Corbet, J.-P. and Mignam, G., Chem. Rev., 2006, vol. 106, p. 2651; Paut, L., Sen, T.K., and Panmiyamurthy, T., Angew. Chem., Int. Ed., 2007, vol. 46, p. 2046.

    Google Scholar 

  4. Dotsenko, V.V., Krivokolysko, S.G., and Litvinov, V.P., Izv. Ross. Akad. Nauk, Ser. Khim., 2007, p. 2397; Xiaozin, B., Zhang, D., Huang, Z., and Yong, Q., Synlett, 2006, p. 3419; Dotsenko, V.V., Krivokolysko, S.G., Rusakov, E.B., Gulov, A.V., and Litvinov, V.P., Khim. Geterotsikl. Soedin., 2007, p. 1075; Dotsenko, V.F., Krivokolysko, S.G., and Litvinov, V.P., Monatsh. Chem., 2007, vol. 138, p. 489; Gonzales-Gomes, J.C., Foubelo, F., and Yus, M., Tetrahedron Lett., 2008, vol. 49, p. 2343.

  5. Mamedbeili, E.G., Dzhafarov, I.A., Kochetkov, K.A., Kyazimova, T.G., Talybov, A.G., and Gasanov, Kh.I., Neftekhimiya, 2009, vol. 49, p. 532; Dzhafarov, I.A., Mamedbeili, E.G., Nagiev, A.V., Gasanov, V.S., and Gasanov, Kh.I., Zh. Prikl. Khim., 2009, vol. 82, p. 322.

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Authors and Affiliations

  1. Mamedaliev Institute of Petrochemical Processes, National Academy of Sciences of Azerbaijan, pr. Khodzhaly 30, Baku, Az, 1025, Azerbaijan

    E. G. Mamedbeili, T. G. Kyazimova & S. T. Alieva

  2. Azerbaijan Pedagogical University, Baku, Azerbaijan

    I. A. Dzhafarov & Kh. I. Gasanov

  3. Nesmeyanov Institute of Organometallic Compounds, Russian Academy of Sciences, ul. Vavilova 28, Moscow, 119991, Russia

    K. A. Kochetkov

Authors
  1. E. G. Mamedbeili
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  2. I. A. Dzhafarov
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  3. K. A. Kochetkov
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  4. T. G. Kyazimova
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  5. Kh. I. Gasanov
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  6. S. T. Alieva
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Corresponding author

Correspondence to E. G. Mamedbeili.

Additional information

Original Russian Text © E.G. Mamedbeili, I.A. Dzhafarov, K.A. Kochetkov, T.G. Kyazimova, Kh.I. Gasanov, S.T. Alieva, 2011, published in Zhurnal Organicheskoi Khimii, 2011, Vol. 47, No. 6, pp. 830–832.

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Mamedbeili, E.G., Dzhafarov, I.A., Kochetkov, K.A. et al. Synthesis of 2-aminomethoxy-1-benzylsulfanylpentanes. Russ J Org Chem 47, 842–844 (2011). https://doi.org/10.1134/S1070428011060029

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  • DOI: https://doi.org/10.1134/S1070428011060029

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