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Synthesis of 20-hydroxyecdysone oxime, its diacetonide, and their 14,15-anhydro derivatives

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Abstract

20-Hydroxyecdysone oxime, its diacetonide, and the corresponding 14,15-anhydro derivatives were synthesized. Conditions were found for the preparation of the Z-and E-oximes, and their characteristics 1H and 13C NMR parameters were determined.

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References

  1. Rodrigues, J., Nunez, L., Peixinho, S., and Jimenez, C., Tetrahedron Lett., 1997, vol. 38, p. 1833.

    Article  Google Scholar 

  2. Holland, H.L., Kumaresan, S., Tan, L., and Njar, V.C.O., J. Chem. Soc., Perkin Trans. 1, 1992, p. 585.

  3. Kovganko, N.V. and Chernov, Yu.G., Khim. Prirodn. Soedin., 2000, p. 149.

  4. Akhrem, A.A. and Kovganko, N.V., Ekdisteroidy: khimiya i biologicheskaya aktivnost’ (Ecdysteroids: Chemistry and Biological Activity), Minsk: Nauka i Tekhnika, 1989.

    Google Scholar 

  5. Afonin, A.V., Ushakov, I.A., Tarasova, O.A., Shmidt, E.Yu., Mikhaleva, A.I., and Voronov, V.K., Russ. J. Org. Chem., 2000, vol. 36, p. 1777.

    CAS  Google Scholar 

  6. Odinokov, V.N., Galyautdinov, I.V., Nedopekin, D.V., Ves’kina, N.A., and Khalilov, L.M., Russ. J. Org. Chem., 2003, vol. 39, p. 952.

    Article  CAS  Google Scholar 

  7. Odinokov, V.N., Savchenko, R.G., Afon’kina, S.R., and Khalilov, L.M., Russ. J. Org. Chem., 2005, vol. 41, p. 376.

    Article  CAS  Google Scholar 

  8. Odinokov, V.N., Savchenko, R.G., Nazmeeva, S.R., Galyautdinov, I.V., and Khalilov, L.M., Russ. Chem. Bull., Int. Ed., 2002, vol. 51, p. 1937.

    Article  CAS  Google Scholar 

  9. Odinokov, V.N., Savchenko, R.G., Nazmeeva, S.R., and Galyautdinov, I.V., Russ. Chem. Bull., Int. Ed., 2002, vol. 51, p. 1963.

    Article  CAS  Google Scholar 

  10. Odinokov, V.N., Galyautdinov, I.V., Nedopekin, D.V., Khalilov, L.M., Shashkov, A.S., Kachala, V.V., Dinan, L., and Lafont, R., Insect Biochem. Molec. Biol., 2002, vol. 32, p. 161.

    Article  CAS  Google Scholar 

  11. Odinokov, V.N., Galyautdinov, I.V., Nedopekin, D.V., and Khalilov, L.M., Russ. Chem. Bull., Int. Ed., 2003, vol. 52, p. 232.

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Institute of Petroleum Chemistry and Catalysis, Russian Academy of Sciences, pr. Oktyabrya 141, Ufa, 450075, Bashkortostan, Russia

    I. V. Galyautdinov, N. A. Ves’kina, S. R. Afon’kina, L. M. Khalilov & V. N. Odinokov

Authors
  1. I. V. Galyautdinov
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  2. N. A. Ves’kina
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  3. S. R. Afon’kina
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  4. L. M. Khalilov
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  5. V. N. Odinokov
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Original Russian Text © I.V. Galyautdinov, N.A. Ves’kina, S.R. Afon’kina, L.M. Khalilov, V.N. Odinokov, 2006, published in Zhurnal Organicheskoi Khimii, 2006, Vol. 42, No. 9, pp. 1352–1357.

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Galyautdinov, I.V., Ves’kina, N.A., Afon’kina, S.R. et al. Synthesis of 20-hydroxyecdysone oxime, its diacetonide, and their 14,15-anhydro derivatives. Russ J Org Chem 42, 1333–1339 (2006). https://doi.org/10.1134/S1070428006090132

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  • DOI: https://doi.org/10.1134/S1070428006090132

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