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Research and development of method for potassium acetate of high purity

  • Inorganic Synthesis and Industrial Inorganic Chemistry
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Abstract

Crystallization of potassium acetate from aqueous solutions, an effect of product yield and washing of its crystals on an efficiency of purification were investigated. Behavior of KCH3COO·1.5H2O was studied in heating. Based on data of the study a technological scheme of producing anhydrous potassium acetate of high purity was developed.

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References

  1. USSR Inventor’s Certificate 1694568.

  2. Savel’ev, E.A. and Pushkov, A.N., Khim.-Farm. Zh., 1986, vol., 20, no. 2, pp. 219–221.

    Google Scholar 

  3. USSR Inventor’s Certificate 1105489.

  4. US Patent 2895990.

  5. Metody polucheniya osobo chistykh neorganicheskikh veshchestv (Techniques of Preparation of Inorganic Substances of High Purity), Stepina, B.D., Gorshteina, I.G., Blyuma, G.Z. et al., Leningrad: Khimiya, 1969.

    Google Scholar 

  6. Spravochnik khimika (Chemist Handbook), Nikol’-skii, B,P., Mosocw; Khimiya.

  7. Krysteva, R.V., Borina, A.F., and Lyashchenko, A.K., Zh. Neorg. Khim., 1985, vol. 30, no. 11, pp. 2957–2962.

    CAS  Google Scholar 

  8. Borina, A.F., Lyashchenko, A.K., and Timofeeva, V.R., Koordinats. Khim., 1984, vol. 10, no. 2, pp., 204–212.

    CAS  Google Scholar 

  9. Popova, S.A., Orlova, V.T., and Borina, A.F., Zh. Neorg. Khim., 1993, vol. 38, no. 4, pp. 717–721.

    CAS  Google Scholar 

  10. Buttgenbach, E., Z. Anorg. Allgem. Chem., 1925, vol. 117, pp. 141–150.

    Article  Google Scholar 

  11. Gasgnier, M. and Petit, A., J. Mater. Sci., 1994, vol. 29, p. 6479.

    Article  CAS  Google Scholar 

  12. Schurman, M. and Huber, F., Acta Cryst., 1994, vol. 50, pp. 1710–1713.

    Google Scholar 

  13. Bryant, R.G., Chacko, V.P., and Etter, M.C., Inorg. Chem., 1984, vol. 23, no. 22, pp. 3520–3584.

    Article  Google Scholar 

  14. Van Niekerk, J.N., Schoening, F.R.L., and Talbot, J.H., Acta Cryst., 1953, vol. 6, pp. 720–723.

    Article  Google Scholar 

  15. Trunov, V.K. and Endeladze, N.O., Zh. Strukt. Khim., 1987, vol. 27, no. 5, pp. 151–153.

    Google Scholar 

  16. Van der Sluis, P., Schouten, A., and Spek, A.L., Acta Cryst., 1987, no. 43, pp., 1922–1924.

  17. Klop, E.A., Schouten, A., and van der Sluis, P., Acta Cryst., 1984, no. 40, pp. 51–53.

  18. Van Niekerk, J.N. and Schoening, F.R.L., Acta Cryst., 1953, vol. 6, pp. 609–612.

    Article  Google Scholar 

  19. Hibbs, D.E., Kolitsch, U., and Leverett, P., Mineral Magazine, 2002, vol. 66, no. 3, pp. 459–464.

    Article  CAS  Google Scholar 

  20. Cameron, T.S., Mannan, K.M., and Rahman, O., Acta Cryst., 1976, no. 32, pp. 87–92.

  21. Chupakhin, M.S., Sukhanovskaya, A.I., Krasil’shchik, V.Z., et al., Metody analiza khimicheskikh reaktivov (Methods of Analysis of Chemical Reagents), Moscow: Khimiya, 1984.

    Google Scholar 

  22. Bouaziz, M.M. and Basset, J.I., Compt. Rend., 1966, no. 265C, pp. 581–585.

  23. Hatibarua, J. and Parry, G.S., Acta Cryst., 1972, no. B28, pp. 3099–3108.

  24. Nirsha, B.M., Chubinidze, A.D., Velikodnyi, Yu.A., et al., Zh. Org. Khim., 1983, vol. 53, no. 7, pp. 1466–1471.

    CAS  Google Scholar 

  25. Gal, S., Meisel, T., Halmos, Z. et al., Magyar Kem. Lapja, 1971, vol. 26, pp. 97–99.

    CAS  Google Scholar 

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Correspondence to A. A. Fakeev.

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Original Russian Text © A.A. Fakeev, G.L. Murskii, V.Z. Krasil’shchik, 2012, published in Zhurnal Prikladnoi Khimii, 2012, Vol. 85, No. 12, pp. 1917–1923.

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Fakeev, A.A., Murskii, G.L. & Krasil’shchik, V.Z. Research and development of method for potassium acetate of high purity. Russ J Appl Chem 85, 1807–1813 (2012). https://doi.org/10.1134/S1070427212120038

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  • DOI: https://doi.org/10.1134/S1070427212120038

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