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Synthesis of 1,3,4-trimethylcyclohex-3-en-1-carboxylic acid allyl ester

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Abstract

The process of diene cyclization of 2,3-dimethylbutadiene with allyl methacrylicate was investigated. Effects of temperature, reaction duration, and ratio of reagents on the yield of 1,3,4-trimethylcyclohex-3-en-1-carboxylic acid allyl ester was studied. Optimal conditions of passing the process were found.

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Authors and Affiliations

  1. Lviv Polytechnical National University, Lviv, Ukraine

    I. S. Polevaya, N. M. Karpyak, M. D. Fedevich, O. I. Marshalok & I. J. Pyrig

Authors
  1. I. S. Polevaya
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  2. N. M. Karpyak
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  3. M. D. Fedevich
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  4. O. I. Marshalok
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  5. I. J. Pyrig
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Additional information

Original Russian Text © I.S. Polevaya, N.M. Karpyak, M.D. Fedevich, O.I. Marshalok, I.J. Pyrig, 2012, published in Zhurnal Prikladnoi Khimii, 2012, Vol. 85, No. 1, pp. 171–173.

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Polevaya, I.S., Karpyak, N.M., Fedevich, M.D. et al. Synthesis of 1,3,4-trimethylcyclohex-3-en-1-carboxylic acid allyl ester. Russ J Appl Chem 85, 164–166 (2012). https://doi.org/10.1134/S107042721201034X

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  • DOI: https://doi.org/10.1134/S107042721201034X

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