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A GLC and NMR analysis of the composition of polyvinyl butyral furfural acetal

  • Macromolecular Compounds and Polymeric Materials
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Abstract

Two procedures were suggested for separate determination of butyral and furfural acetal groups in polyvinyl butyral furfural acetal copolymer. The first procedure involves chromatographic determination of the volatile aldehydes after preliminary hydrolysis of the copolymer, in combination with chemical determination of the sum of acetal groups in the copolymer by oximation. The second procedure is based on NMR spectroscopy.

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Authors and Affiliations

  1. Razuvaev Institute of Organometallic Chemistry, Russian Academy of Sciences, Nizhni Novgorod, Russia

    Yu. A. Kurskii

  2. Kargin Research Institute of Polymer Chemistry and Technology with Pilot Plant, Federal State Unitary Enterprise, Dzerzhinsk, Nizhni Novgorod, Russia

    L. N. Beloded, N. K. Kobyakova, V. N. Kurskaya, K. S. Ludanova, E. P. Pashkina & M. Yu. Ryabinina

  3. Plastpolimer Public Joint-Stock Company, St. Petersburg, Russia

    A. G. Rodionov

Authors
  1. Yu. A. Kurskii
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  2. L. N. Beloded
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  3. N. K. Kobyakova
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  4. V. N. Kurskaya
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  5. K. S. Ludanova
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  6. E. P. Pashkina
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  7. M. Yu. Ryabinina
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  8. A. G. Rodionov
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Additional information

Original Russian Text © Yu.A. Kurskii, L.N. Beloded, N.K. Kobyakova, V.N. Kurskaya, K.S. Ludanova, E.P. Pashkina, M.Yu. Ryabinina, A.G. Rodionov, 2011, published in Zhurnal Prikladnoi Khimii, 2011, Vol. 84, No. 11, pp. 1828–1833.

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Kurskii, Y.A., Beloded, L.N., Kobyakova, N.K. et al. A GLC and NMR analysis of the composition of polyvinyl butyral furfural acetal. Russ J Appl Chem 84, 1914–1919 (2011). https://doi.org/10.1134/S1070427211110139

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  • DOI: https://doi.org/10.1134/S1070427211110139

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