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Synthesis, composition, and properties of products formed in interaction of ortho-tert-butylphenol with sulfur monochloride

  • Organic Synthesis and Industrial Organic Chemistry
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Abstract

Interaction of ortho-tert-butylphenol with sulfur monochloride in dimethylformamide leads to an increase in the fraction of phenol di- and polysulfides in the product. Liquid chromato-mass-spectrometry was used to determine the composition of the main groups of compounds contained in the mixture. A number of its components was isolated and produced by counter synthesis.

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Authors and Affiliations

  1. Vorozhtsov Institute of Organic Chemistry, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russia

    A. P. Krysin, T. G. Egorova, N. I. Komarova, V. G. Vasil’ev & L. M. Pokrovskii

Authors
  1. A. P. Krysin
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  2. T. G. Egorova
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  3. N. I. Komarova
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  4. V. G. Vasil’ev
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  5. L. M. Pokrovskii
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Additional information

Original Russian Text © A.P. Krysin, T.G. Egorova, N.I. Komarova, V.G. Vasil’ev, L.M. Pokrovskii, 2009, published in Zhurnal Prikladnoi Khimii, 2009, Vol. 82, No. 11, pp. 1817–1821.

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Krysin, A.P., Egorova, T.G., Komarova, N.I. et al. Synthesis, composition, and properties of products formed in interaction of ortho-tert-butylphenol with sulfur monochloride. Russ J Appl Chem 82, 1965–1969 (2009). https://doi.org/10.1134/S1070427209110123

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  • DOI: https://doi.org/10.1134/S1070427209110123

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