Abstract
A procedure was developed for preparing perfluoroethanesulfonyl fluoride by synthesis of hexafluoropropane-2-β-sultone from sulfuric anhydride and perfluoropropene, followed by hydrolysis of the sultone to α-tetrafluoroethanesulfonyl fluoride and fluorination of the latter with elemental fluorine.
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Original Russian Text © S.M. Nurgalieva, T.A. Bispen, A.N. Il’in, D.D. Moldavskii, E.A. Rozhkova, 2007, published in Zhurnal Prikladnoi Khimii, 2007, Vol. 80, No. 9, pp. 1529–1532.
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Nurgalieva, S.M., Bispen, T.A., Il’in, A.N. et al. Perfluoroethanesulfonyl fluoride: Preparation from sultone. Russ J Appl Chem 80, 1562–1565 (2007). https://doi.org/10.1134/S1070427207090224
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DOI: https://doi.org/10.1134/S1070427207090224