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Calorimetric and Spectroscopic Studies of Crystallization of Materials

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Abstract

The results of experimental determination of fluorozirconate glass crystallization temperatures by the methods of DSC and spectroscopy have been compared. It has been shown that the crystallization starting temperature, determined by an increase in the light scattering intensity, is 40° below the crystallization point, as seen by DSC. The effect of laser irradiation on the crystallization temperatures of glasses has been detected.

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Authors and Affiliations

  1. Obninsk Institute for Nuclear Power Engineering, National Research Nuclear University, Moscow Engineering Physics Institute, 249040, Obninsk, Russia

    K. V. Klemazov, E. I. Isaev, A. A. Stepanenko & V. A. Stepanov

  2. A.G. Romashin Tekhnologiya Obninsk Research and Production Enterprise, 249031, Obninsk, Russia

    K. V. Klemazov

  3. Interdepartmental Center for Analytical Research in Physics, Chemistry, and Biology under the Presidium of the Russian Academy of Sciences, 117342, Moscow, Russia

    V. A. Stepanov

Authors
  1. K. V. Klemazov
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  2. E. I. Isaev
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  3. A. A. Stepanenko
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  4. V. A. Stepanov
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Correspondence to K. V. Klemazov.

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Klemazov, K.V., Isaev, E.I., Stepanenko, A.A. et al. Calorimetric and Spectroscopic Studies of Crystallization of Materials. Russ J Gen Chem 92, 1148–1152 (2022). https://doi.org/10.1134/S1070363222060299

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  • DOI: https://doi.org/10.1134/S1070363222060299

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