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Tripodal 1,2,3-Triazole Ligands Based on Triphenylphosphine Oxide. Coordination and Extraction Properties

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Abstract

New tripodal 1,2,3-triazole ligands based on triphenylphosphine oxide platform with different linker lengths have been synthesized, and their structure has been determined by elemental analysis, 1H, 13C, and 31P NMR spectroscopy, mass spectrometry, and vibrational (IR and Raman) spectroscopy. The coordination and extraction properties of the new ligands have been studied in the complexation with uranyl nitrate and extraction of micro amounts of uranium(VI) from aqueous phase to 1,2-dichloroethane.

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Funding

TThis work was financially supported by the Russian Science Foundation (project no. 20–13–00329). Spectral studies were carried out using the equipment of the Center for Molecular Structure Studies, Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences.

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Authors and Affiliations

  1. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 119991, Moscow, Russia

    A. G. Matveeva, T. V. Baulina, I. Yu. Kudryavtsev, M. P. Pasechnik, R. R. Aysin, O. V. Bykhovskaya, M. I. Godovikova, S. V. Matveev & V. K. Brel

  2. Institute of Solid State Physics, Russian Academy of Sciences, 142432, Chernogolovka, Russia

    A. N. Turanov

  3. Institute of Microelectronics Technology and High Purity Materials, Russian Academy of Sciences, 142432, Chernogolovka, Russia

    V. K. Karandashev

  4. National University of Science and Technology MISiS, 119991, Moscow, Russia

    V. K. Karandashev

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  1. A. G. Matveeva
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  2. T. V. Baulina
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  3. I. Yu. Kudryavtsev
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  4. M. P. Pasechnik
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  5. R. R. Aysin
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  6. O. V. Bykhovskaya
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  7. M. I. Godovikova
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  8. S. V. Matveev
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  9. A. N. Turanov
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  10. V. K. Karandashev
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  11. V. K. Brel
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Correspondence to A. G. Matveeva.

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Matveeva, A.G., Baulina, T.V., Kudryavtsev, I.Y. et al. Tripodal 1,2,3-Triazole Ligands Based on Triphenylphosphine Oxide. Coordination and Extraction Properties. Russ J Gen Chem 90, 2338–2349 (2020). https://doi.org/10.1134/S107036322012018X

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  • DOI: https://doi.org/10.1134/S107036322012018X

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