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Synthesis of 2,3-Dihydro[1,4]oxazino[2,3,4-ij]quinolinium Bromide and Its Reaction with Sodium Hydroxide

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Abstract

The reaction of quinolin-8-ol with 1,2-dibromoethane in dimethylformamide gave 2,3-dihydro[1,4]-oxazino[2,3,4-ij]quinolinium bromide which reacted with aqueous sodium hydroxide to afford 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4-ij]quinoline, 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4-ij]quinolin-5-ol, and 2,3,4,5-tetrahydro[1,4]oxazino[2,3,4-ij]quinolin-5-one.

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Authors and Affiliations

  1. South Ural State University, pr. Lenina 76, Chelyabinsk, 454080, Russia

    D. G. Kim & A. V. Vasilenko

  2. Chelyabinsk Regional Bureau of Forensic Medical Examination, ul. Varnenskaya 4B, Chelyabinsk, 454076, Russia

    A. B. Melent’ev

Authors
  1. D. G. Kim
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  2. A. V. Vasilenko
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  3. A. B. Melent’ev
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Correspondence to D. G. Kim.

Additional information

Original Russian Text © D.G. Kim, A.V. Vasilenko, A.B. Melent’ev, 2018, published in Zhurnal Obshchei Khimii, 2018, Vol. 88, No. 1, pp. 134–137.

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Kim, D.G., Vasilenko, A.V. & Melent’ev, A.B. Synthesis of 2,3-Dihydro[1,4]oxazino[2,3,4-ij]quinolinium Bromide and Its Reaction with Sodium Hydroxide. Russ J Gen Chem 88, 127–130 (2018). https://doi.org/10.1134/S1070363218010218

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  • DOI: https://doi.org/10.1134/S1070363218010218

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