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Silylation of 2-hydroxypropyl-β-cyclodextrin

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Abstract

The effect of the reaction conditions or the nature of the silylating agents on the silylation of hydroxypropyl-β-cyclodextrin with tert-butyldimethylchloro- and diphenyl-methylchlorosilanes is investigated.

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References

  1. Blum, W. and Aichholz, R., J. High Resol. Chromatogr., 1990, vol. 13, p. 515. doi 10.1002/jhrc.1240130716.

    Article  CAS  Google Scholar 

  2. Maas, B., Dietrich, A., Karl, V., Kaunzinger, A., Lemann, D., Kopke, T., and Mosandl, A., J. Microcol. Sep., 1993, vol. 5, p. 471. doi 10.1002/mcs.1220050505

    Article  Google Scholar 

  3. Zafar, N., Fessi, H., and Elaissari, A., Int. J. Pharm., 2014, vol. 461, p. 351. doi 10.1016/j.ijpharm.2013.12.004

    Article  CAS  Google Scholar 

  4. Farcas, A., Resmerita, A.-M., Stefanache, A., Balan, M., and Harabagiu, V., Beilstein J. Org. Chem., 2012, vol. 8, p. 1505. doi 10.3762/bjoc.8.170

  5. Craft, A.P. and Bartsch, R.A., Tetrahedron, 1983, vol. 39, no. 9, p. 1417. doi 10.1016/S0040-4020(01)88551-3

    Article  Google Scholar 

  6. Khan, A.R., Forgo, P., Stine, K.J., and D’Souza, V.T., Chem. Rev., 1998, vol. 98, no. 5, p. 1977. doi 10.1021/cr970012b

    Article  CAS  Google Scholar 

  7. Crouch, R.D., Tetrahedron, 2013, vol. 69, p. 2383. doi 10.1016/j.tet.2013.01.017

    Article  CAS  Google Scholar 

  8. Kurochkina, G.I., Edunov, A.V., Astakhova, A.G., Grachev, M.K., Levina, I.I., and Nifant’ev, E.E., Russ. J. Gen. Chem., 2013, vol. 83, no. 2, p. 353. doi 10.1134/S1070363213020199

    Article  CAS  Google Scholar 

  9. Kurochkina, G.I., Popkov, A.V., Rasadkina, E.N., and Crachev, M.K., Russ. J. Gen. Chem., 2014, vol. 84, no. 8, p. 1646. doi 10.1134/S1070363214080374

    Article  CAS  Google Scholar 

  10. Cramer, F., Mackensen, G., and Sensse, K., Chem. Ber., 1969, vol. 102, no. 2, p. 494. doi 10.1002/cber.19691020217

    Article  CAS  Google Scholar 

  11. Kurochkina, G.I., Popkov, A.V., Levina, I.I., and Crachev, M.K., Russ. J. Gen. Chem., 2016, vol. 86, no. 2, p. 317. doi 10.1134/S1070363216020195

    Article  CAS  Google Scholar 

  12. Kurochkina, G.I., Popkov, A.V., Rasadkina, E.N., and Crachev, M.K., Russ. J. Gen. Chem., 2014, vol. 84, no. 8, p. 1646. doi 10.1134/S1070363214080374

    Article  CAS  Google Scholar 

  13. Rajewski, R.A. and Stella, V.J., J. Pharm. Sci., 1996, vol. 85, p. 1142. doi 10.1021/is960075u

    Article  CAS  Google Scholar 

  14. Uekama, K., Hirayama, F., and Irie, T., Chem. Rev., 1998, vol. 98, p. 2045. doi 10.1021/cr970025p

    Article  CAS  Google Scholar 

  15. Challa, R., Ahuja, R., Ali, J., and Khar, R.K., AAPS PharmSciTech., 2005, vol. 6, p. E329. doi 10.1208/pt060243

    Article  Google Scholar 

  16. Bricout, H., Leonard, E., Len, C., Landy, D., Hapiot, F., and Monflier, E., Beilstein J. Org. Chem., 2012, vol. 8, p. 1479. doi 10.3762/bjoc.8.167

  17. Memisoglu, E., Bohot, A., Ozalp, M., Sen, M., Duchne, D., and Hincal, A.A., Pharmaceut. Res., 2003, vol. 20, no. 1, p. 117. doi 10.1023/A:1022263111961

    Article  CAS  Google Scholar 

  18. Tiwari, G., Tiwari, R., and Rai, A.K., J. Pharm. Bioallied Sci., 2010, vol. 2, no. 2, p. 72. doi 10.4103/0975-7406.67003

    Article  CAS  Google Scholar 

  19. Raffaini, G., Ganazzoli, F., and Mazzaglia, A., Beilstein J. Org. Chem., 2016, vol. 12, p. 73. doi 10.3762/bjoc.12.8

  20. Kurochkina, G.I., Grachev, M.K., Levina, I.I., and Nifant’ev, E.E., Phosphorus, Sulfur, Silicon, Rel. Elem., 2014, vol. 189, no. 1, p. 33. doi 0.1080/10426507.2013.788006

    Article  CAS  Google Scholar 

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Authors and Affiliations

  1. Moscow Pedagogical State University, Institute of Biology and Chemistry, ul. Kibal’chicha 6/2, Moscow, 129164, Russia

    M. K. Grachev, A. V. Popkov & G. I. Kurochkina

  2. N.M. Emanuel Institute of Biochemical Physics, Russian Academy of Sciences, Moscow, Russia

    I. I. Levina

Authors
  1. M. K. Grachev
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  2. A. V. Popkov
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  3. I. I. Levina
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  4. G. I. Kurochkina
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Corresponding author

Correspondence to A. V. Popkov.

Additional information

Original Russian Text © М.K. Grachev, А.V. Popkov, I.I. Levina, G.I. Kurochkina, 2017, published in Zhurnal Obshchei Khimii, 2017, Vol. 87, No. 7, pp. 1143–1148.

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Grachev, M.K., Popkov, A.V., Levina, I.I. et al. Silylation of 2-hydroxypropyl-β-cyclodextrin. Russ J Gen Chem 87, 1536–1541 (2017). https://doi.org/10.1134/S1070363217070155

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  • DOI: https://doi.org/10.1134/S1070363217070155

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