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Solid-state synthesis of nanocrystalline strontium zirconate assisted by mechanical activation

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Abstract

Nanocrystalline SrZrO3 has been synthesized by a solid-state procedure using mechanical preactivation of a strontium carbonate–zirconia mixture in an AGO-2 centrifugal planetary mill. The effect of mechanical activation of the reactant mixture on the processes occurring during its subsequent heating has been studied by thermal analysis. The resulting strontium zirconate has been characterized by X-ray diffraction and by scanning and transmission electron microscopy.

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Authors and Affiliations

  1. Tananaev Institute of Chemistry and Technology of Rare Elements and Mineral Raw Materials, Kola Science Center, Russian Academy of Sciences, Akademgorodok 26a, Apatity, Murmansk oblast, 184209, Russia

    A. M. Kalinkin, K. V. Balyakin & E. V. Kalinkina

  2. Ioffe Physico-Technical Institute, Russian Academy of Sciences, St. Petersburg, 194021, Russia

    V. N. Nevedomskii

Authors
  1. A. M. Kalinkin
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  2. K. V. Balyakin
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  3. V. N. Nevedomskii
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  4. E. V. Kalinkina
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Correspondence to A. M. Kalinkin.

Additional information

Original Russian Text © A.M. Kalinkin, K.V. Balyakin, V.N. Nevedomskii, E.V. Kalinkina, 2016, published in Zhurnal Obshchei Khimii, 2016, Vol. 86, No. 4, pp. 596–602.

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Kalinkin, A.M., Balyakin, K.V., Nevedomskii, V.N. et al. Solid-state synthesis of nanocrystalline strontium zirconate assisted by mechanical activation. Russ J Gen Chem 86, 785–791 (2016). https://doi.org/10.1134/S1070363216040046

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  • DOI: https://doi.org/10.1134/S1070363216040046

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