Abstract
4,4′-Diaryl-3,3′-spirobi[2-pyrrolidones] were synthesized by hydrogenation of N-substituted 3-methoxycarbonyl-3-(2-nitro-1-arylethyl)-4-phenyl-2-pyrrolidones followed by intramolecular heterocyclization. Structure of the compounds obtained was determined by IR, 1H, and COSY NMR spectroscopy.
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References
Mashkovskii, M.D., Lekarstvennye sredstva (Drugs), Moscow: RIA “Novaya Volna,” 2012.
Berestovitskaya, V.M., Vasil’eva, O.S., and Ostroglyadov, E.S., 2-Pirrolidon i ego proizvodnye (2-Pyrrolidone and Its Derivatives), St. Petersburg: Asterion, 2013.
Berestovitskaya, V.M., Zobacheva, M.M., and Vasil’eva, O.S., Izv. RGPU im. A.I. Gertsena, Ser. Yestestv. i Tochnye Nauki, 2002, no. 2(4), p. 133.
EA Patent no. 002380, 1999; Bull. Izobret. Evraz. Patent. Vedomstva, 2001, no. 1.
Berestovitskaya, V.M., Litvinov, I.A., Vasil’eva, O.S., Nikonorov, A.A., Ostroglyadov, E.S., and Krivolapov, D.B., Russ. Chem. Bull., 2012, vol. 61, no. 5, p. 1014. DOI: 10.1007/s11172-012-0131-5.
Berestovitskaya, V.M., Artemova, O.V., Vasil’eva, O.S., Litvinov, I.A., Gubaidullin, A.T., Krivolapov, D.B., Ostroglyadov, E.S., and Berkova, G.A., Russ. J. Gen. Chem., 2009, vol. 79, no. 4, p. 808. DOI: 10.1134/S1070363209040227.
Artemova, O.V., Vasil’eva, O.S., Ostroglyadov, E.S., Zobacheva, M.M., and Berestovitskaya, V.M., Russ. J. Gen. Chem., 2009, vol. 79, no. 10, p. 2201. DOI: 10.1134/S107036320910020X.
Nikonorov, A.A., Ostroglyadov, E.S., and Vasil’eva, O.S., Russ. J. Gen. Chem., 2011, vol. 81, no. 6, p. 1681. DOI: 10.1134/S1070363211080172.
Ernst, R.R., Bodenhausen, G., and Wokaun, A., Principles of Nuclear Magnetic Resonance in One and Two Dimensions, Oxford: Oxford University Press, 1990.
Claridge, T., Tetrahedron Org. Chem. Ser., 2009, vol. 27, p. 1.
Silverstein, R.M., Webster, F.X., and Kiemle, D., Spectrometric Identification of Organic Compounds, Wiley, 2009.
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Original Russian Text © E.S. Ostroglyadov, O.V. Komarova, O.S. Vasil’eva, N.V. Gorodnicheva, V.M. Berestovitskaya, 2014, published in Zhurnal Obshchei Khimii, 2014, Vol. 84, No. 10, pp. 1663–1666.
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Ostroglyadov, E.S., Komarova, O.V., Vasil’eva, O.S. et al. Synthesis and structure of N-substituted aryl(hetaryl)spiropyrrolidones. Russ J Gen Chem 84, 1941–1944 (2014). https://doi.org/10.1134/S1070363214100144
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DOI: https://doi.org/10.1134/S1070363214100144