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Synthesis of liquid-crystalline 4,4′-dodecyloxybenzoyloxybenzoyl-4-oxy-2-hydroxybenzaldehyde and related azomethine

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Abstract

4,4′-Dodecyloxybenzoyloxybenzoyl-4-hydroxy-2-hydroxybenzaldehyde and the related linear azomethine, the intermediates at the formation of iron(III)-containing complexes, were synthesized. These compounds were characterized by thin layer chromatography, elemental analysis, IR, NMR spectroscopy, mass spectrometry, and by the data of differential scanning calorimetry. The aldehyde and the azomethine show mesomorphic properties.

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Authors and Affiliations

  1. Institute of Solution Chemistry, Russian Academy of Sciences, ul. Academicheskaya 1, Ivanovo, 153045, Russia

    U. V. Chervonova, M. S. Gruzdev & A. M. Kolker

Authors
  1. U. V. Chervonova
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  2. M. S. Gruzdev
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  3. A. M. Kolker
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Corresponding author

Correspondence to M. S. Gruzdev.

Additional information

Original Russian Text © U.V. Chervonova, M.S. Gruzdev, A.M. Kolker, 2011, published in Zhurnal Obshchei Khimii, 2011, Vol. 81, No. 9, pp. 1515–1520.

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Chervonova, U.V., Gruzdev, M.S. & Kolker, A.M. Synthesis of liquid-crystalline 4,4′-dodecyloxybenzoyloxybenzoyl-4-oxy-2-hydroxybenzaldehyde and related azomethine. Russ J Gen Chem 81, 1853 (2011). https://doi.org/10.1134/S1070363211090192

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  • DOI: https://doi.org/10.1134/S1070363211090192

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