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Extraction of fullerene mixture from fullerene soot with organic solvents

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Abstract

Investigation of extraction of fullerene mixture from the fullerene soot obtained by plasma erosion of graphite rod in helium atmosphere with different solvents such as α-chloronaphthalene, o-dichlorobenzene, o-xylene, toluene, benzene, carbon tetrachloride, and n-hexane at 25°C was carried out. Completeness and effectiveness of extraction as well as relative content of light (C60, C70) and heavy (C76, C78, C84) fullerenes in the extract were evaluated.

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References

  1. Williams, H.A., The Most Beautiful Molecule. The Discovery of the Buckyball, John Wiley and Sons, 1997.

  2. Fullerenes, Sidorov, L.N., Ed., Moscow: Ekzamen, 2005.

    Google Scholar 

  3. Ermilov, N.N., Charykov, N.A., Pavlovets, V.A, and Kuznetsova, E.A., Zh. Innovatsii, 2007, vol. 110, no 12, p.79.

    Google Scholar 

  4. Charykov, N.A., Zuev, V.V., and Kuznetsova, E.A., Peterburgskii Zh. Elextroniki, 2007, vol. 53, no. 4, p. 16.

    Google Scholar 

  5. Semenov, K.N., Charykov, N.A., Keskinov, N.A., Piartman, A.K., Blokhin, A.A., and Kopyrin, A.A., J. Chem. Eng. Data, 2010. vol. 55, p. 13.

    Article  CAS  Google Scholar 

  6. Korobov, M.V. and Smith, A.L., Solubility of Fullerenes, Kadish, K.M. and Ruoff, R.S., Eds., John Wiley and Sons, 2000, p. 53.

  7. Storonkin, A.V., Termodinamika geterogennykh system (Thermodynamics of Heterogenic Systems), book 1, pt. 1, 2, 1967, Leningrad: Khimiya.

    Google Scholar 

  8. Semenov, K.N. and Charykov, N.A., J. Chem. Eng. Data, 2010, vol. 55, p. 2373.

    Article  CAS  Google Scholar 

  9. Abdugaev, R.M., Alekhin, O.S., Gerasimov, V.I., Losev, G.M., Nekrasov, K.V., Charykov, N.A., Nikonov, Yu.A, and Soroka, A.I., Russian Patent no. 2256608, 2005.

  10. Abdugaev, R.M., Alekhin, O.S., Gerasimov, V.I., Losev, G.M., Nekrasov, K.V., Charykov, N.A., Nikonov, Yu.A., Soroka, A.I., and Charykov, N.A., Russian Patent no. 39129, 2004.

  11. Kratschmer, W., Lamb, L.D., Fostiropoulos, K., and Huffman, D.R., Nature, 1990, vol. 347, p. 354.

    Article  Google Scholar 

  12. Ponomarev, A.N., Yudovich, M.E., Nikitin, V.A., Nikitin, D.V., Barchenko, V.T., Charykov, N.A., Sobol, V.N., Strel’nikov, K.B., Myshkov, A.I., and Seregin, V.I., Opt. Spectr., 2000, vol. 88, no. 2, p. 195.

    Article  CAS  Google Scholar 

  13. Begak, O.Yu., Metodika opredeleniya kontsentratsii fullerenov metodom zhidkostnoi hromatofrafii (Procedure for Evaluation of Concentration of Fullerenes by Liquid Chromatography), VNIIM im. D.I. Mendeleeva, GOST 8.563-96, attestation MVI no. 242/81-2004.

  14. Spravochnik khimika (Chemist’s Handbook), Nikol’skii, B.P., Leningrad: Khimiya, 1966, vol. 1, p. 617.

    Google Scholar 

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Correspondence to V. A. Keskinov.

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Original Russian Text © L.V. Tsetkova, V.A. Keskinov, N.A. Charykov, N.I. Alekseev, E.G. Gruzinskaya, K.N. Semenov, V.N. Postnov, O.A. Krokhina, 2011, published in Zhurnal Obshchei Khimii, 2011, Vol. 81, No. 5, pp. 832–839.

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Tsetkova, L.V., Keskinov, V.A., Charykov, N.A. et al. Extraction of fullerene mixture from fullerene soot with organic solvents. Russ J Gen Chem 81, 920–926 (2011). https://doi.org/10.1134/S1070363211050136

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  • DOI: https://doi.org/10.1134/S1070363211050136

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