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Synthesis and structure of bis[1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dionato]copper

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Abstract

Previously unknown 1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dione and its copper complex, bis [1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dionato]copper, were synthesized. The 1H NMR, IR, and ESR spectra and X-ray diffraction patterns of the synthesized compounds were obtained. Volatilily and thermal stability of the copper complex were studied by thermogravimetric analysis and differential scanning calorimetry.

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Authors and Affiliations

  1. Razuvaev Institute of Organometallic Chemistry, Russian Academy of Sciences, ul. Tropinina 49, Nizhny Novgorod, 603600, Russia

    V. K. Khamylov, T. S. Pochekutova, B. I. Petrov, M. V. Sizov, G. K. Fukin, Yu. A. Kurskii & A. V. Arapova

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  1. V. K. Khamylov
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  2. T. S. Pochekutova
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  3. B. I. Petrov
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  4. M. V. Sizov
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  5. G. K. Fukin
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  6. Yu. A. Kurskii
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  7. A. V. Arapova
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Correspondence to V. K. Khamylov.

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Original Russian Text © V.K. Khamylov, T.S. Pochekutova, B.I. Petrov, M.V. Sizov, G.K. Fukin, Yu.A. Kurskii, A.V. Arapova, 2009, published in Zhurnal Obshchei Khimii, 2009, Vol. 79, No. 1, pp. 33–38.

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Khamylov, V.K., Pochekutova, T.S., Petrov, B.I. et al. Synthesis and structure of bis[1-(1-adamantyl)-4,4,4-trifluorobutane-2,4-dionato]copper. Russ J Gen Chem 79, 31–36 (2009). https://doi.org/10.1134/S1070363209010058

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  • DOI: https://doi.org/10.1134/S1070363209010058

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