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Features of phosphorylation of Per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin with a phosphorous diamidoester

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Abstract

Phosphorylation of secondary hydroxy groups in per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin with a phosphorous diamidoester is found to proceed, unlike phosphorylation of free β-cyclodextrin, at an elevated temperature and is accompanied by substantial desilylation.

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Authors and Affiliations

  1. Moscow Pedagogical State University, Nesvizhskii per. 3, Moscow, 119021, Russia

    G. I. Kurochkina, I. A. Senyushkina, M. K. Grachev, L. K. Vasyanina & E. E. Nifant’ev

Authors
  1. G. I. Kurochkina
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  2. I. A. Senyushkina
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  3. M. K. Grachev
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  4. L. K. Vasyanina
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  5. E. E. Nifant’ev
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Correspondence to G. I. Kurochkina.

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Original Russian Text © G.I. Kurochkina, I.A. Senyushkina, M.K. Grachev, L.K. Vasyanina, E.E. Nifant’ev, 2008, published in Zhurnal Obshchei Khimii, 2008, Vol. 78, No. 1, pp. 64–67.

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Kurochkina, G.I., Senyushkina, I.A., Grachev, M.K. et al. Features of phosphorylation of Per-6-O-(tert-butyldimethylsilyl)-β-cyclodextrin with a phosphorous diamidoester. Russ J Gen Chem 78, 61–64 (2008). https://doi.org/10.1134/S1070363208010118

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  • DOI: https://doi.org/10.1134/S1070363208010118

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