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Dichlorophosphate anion in the synthesis of thioamides

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Abstract

Phosphorus thiochloride reaction with dimethylformamide and dimethylacetamide leading to corresponding thioamides is studied. The thionylating agent is dichlorothiophosphate anion generated in the reaction course.

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Original Russian Text © S.E. Pipko, N.V. Simurova, V.V. Shvadchak, L.V. Bezgubenko, S.N. Luk’yanenko, 2006, published in Zhurnal Obshchei Khimii, 2006, Vol. 76, No. 7, pp. 1065–1067.

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Pipko, S.E., Simurova, N.V., Shvadchak, V.V. et al. Dichlorophosphate anion in the synthesis of thioamides. Russ J Gen Chem 76, 1019–1021 (2006). https://doi.org/10.1134/S1070363206070036

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  • DOI: https://doi.org/10.1134/S1070363206070036

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