Skip to main content
SpringerLink
Log in

1H NMR spectra and crystal structure of the nickel(II) complex with ethyl 5,5-dimethyl-2,4-dioxohexanoate aroylhydrazones

  • Published:
Russian Journal of Coordination Chemistry Aims and scope Submit manuscript

Abstract

Nickel(II) complexes NiLn ∙ NH3 (n = 1–5) with the products of condensation of ethyl 5,5-dimethyl-2,4-dioxohexanoate with aromatic acid hydrazides (H2L1–H2L5) were synthesized. The complexes were studied by elemental analysis and IR and 1H NMR spectroscopy. The structure of the complex NiL1 ∙ NH3 was determined by X-ray diffraction (CIF file CCDC no. 1057268).

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. Parpiev, N.A., Yusupov, S.I., Yakimovich, S.I., and Sharipov, Kh.T., Atsilgidrazony i ikh kompleksy s perekhodnymi metallami (Acylhydrazones and Their Complexes with Transition Metals), Tashkent Fan, 1988.

    Google Scholar 

  2. Sovremennye problemy sinteza i issledovaniya organicheskikh soedinenii (Modern Problems of Synthesis and Study of Organic Compounds), Kostikov, R.R., Ed., Leningrad Leningrad. Gos. Univ., 1990.

  3. Yakimovich, S.I. and Zerova, I.V., Zh. Org. Khim., 1991, vol. 27, no. 5, p. 959.

    CAS  Google Scholar 

  4. Yakimovich, S.I. and Nikolaev, V.N., Zh. Org. Khim., 1981, vol. 17, no. 2, p. 284.

    CAS  Google Scholar 

  5. Yakimovich, S.I., Nikolaev, V.N., and Zerova, I.V., Zh. Org. Khim., 1986, vol. 22, no. 2, p. 286.

    CAS  Google Scholar 

  6. Umarov, B.B., Doctoral (Chem.) Dissertation, Tashkent IU ANRUz., 1996.

    Google Scholar 

  7. Tursunov, M.A., Avezov, K.G., Abdurakhmonov, S.F., et al., Materialy Respublikanskoi nauchno-prakticheskoi konferentsii “Aktual’nye problemy khimicheskoi tekhnologii” (Proc. Republican Sci. Pract. Conf. “Modern Problems of Chemical Engineering”), Bukhara: BukhITI, 2014, p. 34.

    Google Scholar 

  8. Tursunov, M.A., Umarov, B.B., Avezov, K.G., et al., Trudy Mezhdunar. simpoziuma po fundamental’nym i prikladnym problemam nauki (Proc. Int. Symp. on Fundamental and Applied Problems of Science), Moscow, 2013, vol. 1, ch. 8., p. 158.

    Google Scholar 

  9. Tursunov, M.A., Umarov, B.B., Avezov, K.G., et al., Sb. materialov XVIII Mezhdunar. nauch.-prakt. konf. “Fundamental’nye i prikladnye issledovaniya: problemy i rezul’taty” (Proc. XVIII Int. Sci. Pract. Conf. “Fundamental and Applied Research: Problems and Results”) Novosibirsk, 2015, p. 151.

    Google Scholar 

  10. Tursunov, M.A., Umarov, B.B., Minin, V.V., et al., Abstracts of Papers, Respubl. nauch.-tekhn. konf. “Sovremennye tekhnologii i innovatsii gorno-metallurgicheskoi otrasli” (Republ. Sci. and Technol. Conf. “Modern Technologies and Innovations of Ore Mining and Smelting Industry”), Navoi: NavGGI, 2012, p. 350.

    Google Scholar 

  11. Umarov, B.B., Toshev, M.T., Yakimovich, S.I., et al., Koord. Khim., 1992, vol. 18, no. 9, p. 980.

    CAS  Google Scholar 

  12. Tursunov, M.A., Avezov, K.G., Umarov, B.B., and Parpiev, N.A., Materialy Mezhdunar. nauch.-prakt. konf. “Aktual’nye problemy otraslei khimicheskoi tekhnologii” (Proc. Int. Sci. and Pract. Conf. “Modern Problems of Chemical Engineering Branches”) Bukhara: BukhITI, 2015, p. 237.

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Bukhara State University, Bukhara, Uzbekistan

    M. A. Tursunov, K. G. Avezov, B. B. Umarov & N. A. Parpiev

Authors
  1. M. A. Tursunov
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. K. G. Avezov
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. B. B. Umarov
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. N. A. Parpiev
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to M. A. Tursunov.

Additional information

Original Russian Text © M.A. Tursunov, K.G. Avezov, B.B. Umarov, N.A. Parpiev, 2017, published in Koordinatsionnaya Khimiya, 2017, Vol. 43, No. 2, pp. 99–102.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Tursunov, M.A., Avezov, K.G., Umarov, B.B. et al. 1H NMR spectra and crystal structure of the nickel(II) complex with ethyl 5,5-dimethyl-2,4-dioxohexanoate aroylhydrazones. Russ J Coord Chem 43, 93–96 (2017). https://doi.org/10.1134/S1070328417020087

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S1070328417020087

Keywords

Search

Navigation