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Synthesis, characterization, and X-ray crystal structures of oxovanadium(V) complexes with hydrazone and 8-hydroxyquinoline ligands

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Abstract

Three new oxovanadium(V) complexes with the general formula [VO(L)n(HQ)] (n = 1–3) were prepared by the reaction of [VO(Acac)2] (Acac = acetylacetonate) and 8-hydroxyquinoline with similar benzohydrazide ligands in methanol. Crystal and molecular structures of the complexes were determined by elemental analysis, infrared and UV-Vis spectra and single crystal X-ray diffraction (CIF file CCDC nos. 1004087 (I), 1004088 (II), and 1004089 (III)). The V atoms are in octahedral coordination. Thermal stability of the complexes were studied.

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Authors and Affiliations

  1. School of Life Sciences, Shandong University of Technology, Zibo, 25504, P.R. China

    S. S. Qian & H. L. Zhu

  2. Department of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian, 116029, P.R. China

    Y. T. Ye, J. Q. Ren & Z. You

Authors
  1. S. S. Qian
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  2. Y. T. Ye
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  3. J. Q. Ren
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  4. Z. You
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  5. H. L. Zhu
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Correspondence to Z. You.

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Qian, S.S., Ye, Y.T., Ren, J.Q. et al. Synthesis, characterization, and X-ray crystal structures of oxovanadium(V) complexes with hydrazone and 8-hydroxyquinoline ligands. Russ J Coord Chem 40, 948–953 (2014). https://doi.org/10.1134/S1070328414120112

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  • DOI: https://doi.org/10.1134/S1070328414120112

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