Abstract
It is shown that the use of the dynamic light scattering (DLS) method for determining nanoparticle dimensions in sols containing mixtures of particles with various sizes may lead to incorrect results, since the distribution of small particle sizes can remain unrecognized. The conditions and threshold of this phenomenon are established. It is indicated that the measurement of nanoparticle dimensions by DLS in these cases must be supplemented by auxiliary optical measurements.
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References
A. Ya. Vul’, A. T. Dideikin, Z. G. Tsareva, M. N. Korytov, P. N. Brunkov, B. G. Zhukov, and S. I. Rozov, Tech. Phys. Lett. 32, 561 (2006).
A. I. Shames, A. M. Panich, W. Kempinski, A. E. Aleksenskiy, M. V. Baidakova, A. T. Dideikin, V. Yu. Osipov, V. I. Siklitsky, E. Osawa, M. Ozawa, and A. Ya. Vull’, J. Phys. Chem. Solids 63, 1993 (2002).
V. L. Kuznetsov, A. L. Chuvilin, Yu. V. Butenko, I. Yu. Malkov, and V. M. Titov, Chem. Phys. Lett. 224, 343 (1994).
A. M. Schrand, S. A. C. Hens, and O. A. Shenderova, Crit. Rev. Solid State Mater. Sci. 34, 18 (2009).
B. J. Berne and R. Pecora, Dynamic Light Scattering (Wiley, New York, 1976).
O. A. Williams, J. Hees, C. Dieker, W. Jäder, W. Kirste, and C. E. Nebel, ACS Nano 4, 4824 (2010).
A. F. Aleksenskiy E. D. Eydelman, and A. Ya. Vul’, Nanosci. Nanotechnol. Lett. 3, 68 (2011).
A. E. Aleksenskii, A. Ya. Vul’, and M. A. Yagovkina, Method of Nanodiamond Purification, RF Patent no. 2322389 (20.04.2008, priority of 13.10.2006).
A. E. Aleksenskii, M. V. Baidakova, A. I. Veinger, A. Ya. Vul’, S. P. Vul’, and M. A. Yagovkina, Method of Magnetic Impurity Control in Detonation Nanodiamonds, RF Patent No. 2388688 (10.05.2010, priority of 16.16.10.2008).
A. Ya. Vul’, in Ultrananocrystalline Diamond: Synthesis, Properties, and Applications, Ed. by O. A. Shenderova and D. M. Gruen (William Andrew, Norwich, NY, 2006), pp. 379–404.
Y. D. Yan and J. H. R. Clarke, Adv. Colloid Interface Sci. 29, 277 (1989).
A. E. Aleksenskii, A. Ya. Vul’, S. V. Konyakhin, K. V. Reikh, L. V. Sharonova, and E. D. Eidel’man, Phys. Solid State 54, 578 (2012).
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Original Russian Text © A.E. Aleksenskii, A.V. Shvidchenko, E.D. Eidel’man, 2012, published in Pis’ma v Zhurnal Tekhnicheskoi Fiziki, 2012, Vol. 38, No. 23, pp. 1–10.
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Aleksenskii, A.E., Shvidchenko, A.V. & Eidel’man, E.D. The applicability of dynamic light scattering to determination of nanoparticle dimensions in sols. Tech. Phys. Lett. 38, 1049–1052 (2012). https://doi.org/10.1134/S1063785012120024
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DOI: https://doi.org/10.1134/S1063785012120024
Keywords
- Electron Paramagnetic Resonance
- Dynamic Light Scattering
- Dynamic Light Scattering
- Technical Physic Letter
- Scattered Light Intensity