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Blazed Silicon Gratings for Soft X-Ray and Extreme Ultraviolet Radiation: the Effect of Groove Profile Shape and Random Roughness on the Diffraction Efficiency

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Abstract

The effect of the groove profile shape and random roughness of the reflecting facet of five silicon diffraction gratings (1°–4° blaze angle, period 0.4, 1.4, 2, and 4 μm, various coatings) operating in the soft X-ray and extreme ultraviolet radiation ranges on the outflow of the diffraction efficiency from working orders is studied. Diffraction gratings were fabricated by wet etching of Si(111) vicinal wafers and characterized by atomic force microscopy to determine the shape of the groove profile and roughness. The diffraction efficiency of gratings operating in classical and conical diffraction mounts was calculated based on realistic groove profiles by computer simulation using the PCGrateTM code and taking into account the scattering intensity using Nevot–Croce or Debye–Waller corrections or using the Monte Carlo method (rigorously). The effect ofthe groove profile shape and roughness on the diffraction efficiency of the fabricated Si gratings is shown.

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REFERENCES

  1. L. I. Goray, G. Schmidt. In: Gratings: Theory and Numerical Applications, ed. by E. Popov (Institut Fresnel, AMU, 2014), p. 447.

  2. L. Goray, M. Lubov. J. Appl. Cryst., 46, 926 (2013). https://doi.org/10.1107/S0021889813012387

    Article  ADS  CAS  Google Scholar 

  3. L. I. Goray, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov, A. V. Nashchekin, M. V. Zorina, M. M. Barysheva, S. A. Garakhin, S. Yu. Zuev, N. I. Chkhalo. Bull. of the Lebedev Phys. Inst. 50 (2), S250 (2023). https:// link.springer.com/article/10.3103/S1068335623140063.

    Article  ADS  Google Scholar 

  4. L. I. Goray. J. Appl. Phys., 108, 033516 (2010). https://doi.org/10.1063/1.3467937

  5. D. L. Voronov, E. H. Anderson, R. Cambie, F. Salmassi, E. M. Gullikson, V. V. Yashchuk, H. A. Padmore, M. Ahn, C.-H. Chang, R. K. Heilmann, M. L. Schattenburg. Proc. SPIE, 7448, 74480J (2009). https://doi.org/10.1117/12.826921

  6. L. Golub, P. Cheimets, E. E. DeLuca, C. A. Madsen, K. K. Reeves, J. Samra, S. Savage, A. Winebarger, A. R. Bruccoleri. J. Space Weather Space Clim., 10, 37 (2020). https://doi.org/10.1051/swsc/2020040

    Article  ADS  Google Scholar 

  7. L. I. Goray, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov. Tech. Phys., 92 (13), 2097 (2022). https://doi.org/10.21883/JTF.2021.10.51368.81-21

    Article  Google Scholar 

  8. D. V. Mokhov, T. N. Berezovskaya, K. Yu. Shubina, E. V. Pirogov, A. V. Nashchekin, V. A. Sharov, L. I. Goray, Tech. Phys., 92 (8), 1009 (2022). https://doi.org/10.21883/JTF.2022.08.52782.74-22

    Article  Google Scholar 

  9. L. Goray, M. Lubov. J. Surf. Invest. X-ray Synchrotron Neutron Tech., 8 (3), 444 (2014). https://doi.org/10.1134/S1027451014030057

    Article  CAS  Google Scholar 

  10. L. Goray, M. Lubov. Opt. Express, 23 (8), 10703 (2015). https://doi.org/10.1364/OE.23.010703

    Article  ADS  CAS  PubMed  Google Scholar 

  11. J. A. Ogilvy. Rep. Prog. Phys., 50, 1553 (1987). https://doi.org/10.1088/0034-4885/50/12/001

    Article  ADS  MathSciNet  Google Scholar 

  12. D. K. G. de Boer. Phys. Rev. B, 51, 5297 (1995). https://doi.org/10.1103/PhysRevB.51.5297

    Article  ADS  CAS  Google Scholar 

  13. D. G. Stearns, D. P. Gaines, D. W. Sweeney, E. M. Gullikson. J. Appl. Phys., 84 (2), 1003 (1998). https://doi.org/10.1063/1.368098

    Article  ADS  CAS  Google Scholar 

  14. I. V. Kozhevnikov, M. V. Pyatakhin. J. X-ray Sci. Tech., 8(4), 253 (1998).

    Google Scholar 

  15. M. Saillard, D. Maystre, J. P. Rossi. Opt. Acta, 33, 1193 (1986).

    Article  ADS  CAS  Google Scholar 

  16. L. I. Goray Nucl. Instrum. Methods. Phys. Res. A, 536 (1–2), 211 (2005). https://doi.org/10.1016/j.nima.2004.07.173

  17. L. Goray. Proc. SPIE, 6617, 661719 (2007). https://doi.org/10.1117/12.726038

  18. L. Goray. Proc. SPIE, 7390, 73900V (2009). https://doi.org/10.1117/12.827444

  19. L. I. Goray, E. V. Pirogov, M. S. Sobolev, N. K. Polyakov, A. S. Dashkov, M. V. Svechnikov, A. D. Bouravleuv. Tech. Phys., 65 (11), 1822 (2020). https://doi.org/10.1134/S1063784220110134

    Article  Google Scholar 

  20. L. Goray, E. Pirogov, M. Sobolev, I. Ilkiv, A. Dashkov, E. Nikitina, E. Ubyivovk, L. Gerchikov, A. Ipatov, Yu. Vainer, M. Svechnikov, P. Yunin, N. Chkhalo, A. Bouravlev. J. Phys. D: Appl. Phys., 53, 455103 (2020).]https://doi.org/10.1088/1361-6463/aba4d6

  21. L. Goray. J. Synchrotron Radiat., 28, 196 (2021). https://doi.org/10.1107/S160057752001440X

    Article  CAS  PubMed  Google Scholar 

  22. I. I. G., Inc. [Electronic source]. Available at: URL: http://pcgrate.com, open access (date of access: 03.06.2023).

  23. L. I. Goray, N. I. Chkhalo, Yu. A. Vainer, Tech. Phys. Let., 36 (2), 108 (2010). https://doi.org/10.1134/S1063785010020057

    Article  CAS  Google Scholar 

  24. L. I. Goray, N. I. Chkhalo, G. E. Tsyrlin. Tech. Phys., 54, 561 (2009). https://doi.org/10.1134/S1063784209040185

    Article  CAS  Google Scholar 

  25. L. I. Goray, E. V. Pirogov, M. V. Svechnikov, M. S. Sobolev, N. K. Polyakov, L. G. Gerchikov, E. V. Nikitina, A. S. Dashkov, M. M. Borisov, S. N. Yakunin, A. D. Bouravleuv. Tech. Phys. Lett., 47 (10), 757 (2021). https://doi.org/10.1134/S1063785021080071

    Article  ADS  CAS  Google Scholar 

  26. M. Lubov, L. Goray. J. Synchrotron Rad., 26, 1539 (2019). https://doi.org/10.1107/S1600577519006337

    Article  CAS  Google Scholar 

  27. L. I. Goray, V. E. Asadchikov, B. S. Roshchin, Yu. O. Volkov, A. M. Tikhonov. OSA Continuum, 2(2), 460 (2019). https://doi.org/10.1364/OSAC.2.000460

    Article  CAS  Google Scholar 

  28. L. I. Goray, J. F. Seely. Appl. Opt., 41 (7), 1434 (2002). https://doi.org/10.1364/AO.41.001434

    Article  ADS  PubMed  Google Scholar 

  29. L. I. Gorai, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov. Poverkhn.: Rentgenovskie, Sinkhrotronnye Neitr. Issled., 8, 3 (2023) (in Russian).

    Google Scholar 

  30. Gwyddion download [Electronic source]. Available at: http://gwyddion.net/download.php, open access (date of access: 05.22.2023).

  31. L. I. Goray, In: Recent Developments in Atomic Force Microscopy and Raman Spectroscopy for Materials Characterization, ed. by C. S. Pathak, S. Kumar (IntechOpen, 2022), 274 p. https://doi.org/10.5772/intechopen.94185

    Book  Google Scholar 

  32. L. Goray, W. Jark, D. Eichert. J. Synchrotron Radiat., 25, 1683 (2018). https://doi.org/10.1107/S1600577518012419

    Article  PubMed  Google Scholar 

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Funding

The experimental work of L.I. Goray, A.S. Dashkov, D.V. Mokhov, E.V. Pirogov, and K.Yu. Shubina was supported by the Russian Science Foundation (19-12-00270-P). Numerical calculations were carried out with support from the Russian Foundation for Basic Research (19-29-12053-mk).

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Goray, L.I., Sharov, V.A., Mokhov, D.V. et al. Blazed Silicon Gratings for Soft X-Ray and Extreme Ultraviolet Radiation: the Effect of Groove Profile Shape and Random Roughness on the Diffraction Efficiency. Tech. Phys. 68 (Suppl 1), S51–S58 (2023). https://doi.org/10.1134/S1063784223090062

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