Abstract
The effect of the groove profile shape and random roughness of the reflecting facet of five silicon diffraction gratings (1°–4° blaze angle, period 0.4, 1.4, 2, and 4 μm, various coatings) operating in the soft X-ray and extreme ultraviolet radiation ranges on the outflow of the diffraction efficiency from working orders is studied. Diffraction gratings were fabricated by wet etching of Si(111) vicinal wafers and characterized by atomic force microscopy to determine the shape of the groove profile and roughness. The diffraction efficiency of gratings operating in classical and conical diffraction mounts was calculated based on realistic groove profiles by computer simulation using the PCGrateTM code and taking into account the scattering intensity using Nevot–Croce or Debye–Waller corrections or using the Monte Carlo method (rigorously). The effect ofthe groove profile shape and roughness on the diffraction efficiency of the fabricated Si gratings is shown.
REFERENCES
L. I. Goray, G. Schmidt. In: Gratings: Theory and Numerical Applications, ed. by E. Popov (Institut Fresnel, AMU, 2014), p. 447.
L. Goray, M. Lubov. J. Appl. Cryst., 46, 926 (2013). https://doi.org/10.1107/S0021889813012387
L. I. Goray, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov, A. V. Nashchekin, M. V. Zorina, M. M. Barysheva, S. A. Garakhin, S. Yu. Zuev, N. I. Chkhalo. Bull. of the Lebedev Phys. Inst. 50 (2), S250 (2023). https:// link.springer.com/article/10.3103/S1068335623140063.
L. I. Goray. J. Appl. Phys., 108, 033516 (2010). https://doi.org/10.1063/1.3467937
D. L. Voronov, E. H. Anderson, R. Cambie, F. Salmassi, E. M. Gullikson, V. V. Yashchuk, H. A. Padmore, M. Ahn, C.-H. Chang, R. K. Heilmann, M. L. Schattenburg. Proc. SPIE, 7448, 74480J (2009). https://doi.org/10.1117/12.826921
L. Golub, P. Cheimets, E. E. DeLuca, C. A. Madsen, K. K. Reeves, J. Samra, S. Savage, A. Winebarger, A. R. Bruccoleri. J. Space Weather Space Clim., 10, 37 (2020). https://doi.org/10.1051/swsc/2020040
L. I. Goray, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov. Tech. Phys., 92 (13), 2097 (2022). https://doi.org/10.21883/JTF.2021.10.51368.81-21
D. V. Mokhov, T. N. Berezovskaya, K. Yu. Shubina, E. V. Pirogov, A. V. Nashchekin, V. A. Sharov, L. I. Goray, Tech. Phys., 92 (8), 1009 (2022). https://doi.org/10.21883/JTF.2022.08.52782.74-22
L. Goray, M. Lubov. J. Surf. Invest. X-ray Synchrotron Neutron Tech., 8 (3), 444 (2014). https://doi.org/10.1134/S1027451014030057
L. Goray, M. Lubov. Opt. Express, 23 (8), 10703 (2015). https://doi.org/10.1364/OE.23.010703
J. A. Ogilvy. Rep. Prog. Phys., 50, 1553 (1987). https://doi.org/10.1088/0034-4885/50/12/001
D. K. G. de Boer. Phys. Rev. B, 51, 5297 (1995). https://doi.org/10.1103/PhysRevB.51.5297
D. G. Stearns, D. P. Gaines, D. W. Sweeney, E. M. Gullikson. J. Appl. Phys., 84 (2), 1003 (1998). https://doi.org/10.1063/1.368098
I. V. Kozhevnikov, M. V. Pyatakhin. J. X-ray Sci. Tech., 8(4), 253 (1998).
M. Saillard, D. Maystre, J. P. Rossi. Opt. Acta, 33, 1193 (1986).
L. I. Goray Nucl. Instrum. Methods. Phys. Res. A, 536 (1–2), 211 (2005). https://doi.org/10.1016/j.nima.2004.07.173
L. Goray. Proc. SPIE, 6617, 661719 (2007). https://doi.org/10.1117/12.726038
L. Goray. Proc. SPIE, 7390, 73900V (2009). https://doi.org/10.1117/12.827444
L. I. Goray, E. V. Pirogov, M. S. Sobolev, N. K. Polyakov, A. S. Dashkov, M. V. Svechnikov, A. D. Bouravleuv. Tech. Phys., 65 (11), 1822 (2020). https://doi.org/10.1134/S1063784220110134
L. Goray, E. Pirogov, M. Sobolev, I. Ilkiv, A. Dashkov, E. Nikitina, E. Ubyivovk, L. Gerchikov, A. Ipatov, Yu. Vainer, M. Svechnikov, P. Yunin, N. Chkhalo, A. Bouravlev. J. Phys. D: Appl. Phys., 53, 455103 (2020).]https://doi.org/10.1088/1361-6463/aba4d6
L. Goray. J. Synchrotron Radiat., 28, 196 (2021). https://doi.org/10.1107/S160057752001440X
I. I. G., Inc. [Electronic source]. Available at: URL: http://pcgrate.com, open access (date of access: 03.06.2023).
L. I. Goray, N. I. Chkhalo, Yu. A. Vainer, Tech. Phys. Let., 36 (2), 108 (2010). https://doi.org/10.1134/S1063785010020057
L. I. Goray, N. I. Chkhalo, G. E. Tsyrlin. Tech. Phys., 54, 561 (2009). https://doi.org/10.1134/S1063784209040185
L. I. Goray, E. V. Pirogov, M. V. Svechnikov, M. S. Sobolev, N. K. Polyakov, L. G. Gerchikov, E. V. Nikitina, A. S. Dashkov, M. M. Borisov, S. N. Yakunin, A. D. Bouravleuv. Tech. Phys. Lett., 47 (10), 757 (2021). https://doi.org/10.1134/S1063785021080071
M. Lubov, L. Goray. J. Synchrotron Rad., 26, 1539 (2019). https://doi.org/10.1107/S1600577519006337
L. I. Goray, V. E. Asadchikov, B. S. Roshchin, Yu. O. Volkov, A. M. Tikhonov. OSA Continuum, 2(2), 460 (2019). https://doi.org/10.1364/OSAC.2.000460
L. I. Goray, J. F. Seely. Appl. Opt., 41 (7), 1434 (2002). https://doi.org/10.1364/AO.41.001434
L. I. Gorai, T. N. Berezovskaya, D. V. Mokhov, V. A. Sharov, K. Yu. Shubina, E. V. Pirogov, A. S. Dashkov. Poverkhn.: Rentgenovskie, Sinkhrotronnye Neitr. Issled., 8, 3 (2023) (in Russian).
Gwyddion download [Electronic source]. Available at: http://gwyddion.net/download.php, open access (date of access: 05.22.2023).
L. I. Goray, In: Recent Developments in Atomic Force Microscopy and Raman Spectroscopy for Materials Characterization, ed. by C. S. Pathak, S. Kumar (IntechOpen, 2022), 274 p. https://doi.org/10.5772/intechopen.94185
L. Goray, W. Jark, D. Eichert. J. Synchrotron Radiat., 25, 1683 (2018). https://doi.org/10.1107/S1600577518012419
Funding
The experimental work of L.I. Goray, A.S. Dashkov, D.V. Mokhov, E.V. Pirogov, and K.Yu. Shubina was supported by the Russian Science Foundation (19-12-00270-P). Numerical calculations were carried out with support from the Russian Foundation for Basic Research (19-29-12053-mk).
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Goray, L.I., Sharov, V.A., Mokhov, D.V. et al. Blazed Silicon Gratings for Soft X-Ray and Extreme Ultraviolet Radiation: the Effect of Groove Profile Shape and Random Roughness on the Diffraction Efficiency. Tech. Phys. 68 (Suppl 1), S51–S58 (2023). https://doi.org/10.1134/S1063784223090062
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DOI: https://doi.org/10.1134/S1063784223090062