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Self-Organization of a Bioactive Nanostructured Oxide Layer at the Surface of Sintered Titanium Sponge Powder Subjected to Electrochemical Anodization

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Abstract

Self-ordered nanoporous/nanotubular oxide films are prepared on the surface of porous powder materials of a titanium sponge by electrochemical anodization. By using scanning electron and atomic force microscopies, we establish that anodization of sintered powder of a titanium sponge in an electrolyte containing H2SO4 (10%) and HF (0.15%) yields an X-ray amorphous TiO2 film with a thickness of 250–350 nm and a regular pattern of nanopores and nanotubes with diameters of 30 to 70 nm. Our results confirm that the described method for surface modification of sintered powders of a titanium sponge holds promise in manufacturing bioactive implants.

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ACKNOWLEDGMENTS

The work was supported by the Russian Foundation for Basic Research, project no. 15-58-04086 Bel_mol_a and the Belarusian Republican Foundation for Fundamental Research, agreement T15RM-062.

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Authors and Affiliations

  1. Petrozavodsk State University, 185910, Petrozavodsk, Russia

    A. N. Kokatev, K. V. Stepanova, N. M. Yakovleva & A. M. Shul’ga

  2. Powder Metallurgy Institute, 220005, Minsk, Belorussia

    V. E. Tolstik & A. I. Shelukhina

Authors
  1. A. N. Kokatev
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  2. K. V. Stepanova
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  3. N. M. Yakovleva
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  4. V. E. Tolstik
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  5. A. I. Shelukhina
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  6. A. M. Shul’ga
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Corresponding author

Correspondence to N. M. Yakovleva.

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Translated by A. Kukharuk

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Kokatev, A.N., Stepanova, K.V., Yakovleva, N.M. et al. Self-Organization of a Bioactive Nanostructured Oxide Layer at the Surface of Sintered Titanium Sponge Powder Subjected to Electrochemical Anodization. Tech. Phys. 63, 1334–1340 (2018). https://doi.org/10.1134/S1063784218090062

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