Abstract
The magnetic properties of magnesium–iron spinel (MgFe2O4) powdered nanoparticles obtained by glycine–nitrate synthesis are investigated by X-ray phase analysis and the NMR method. According to the results of X-ray phase analysis, the average size of the crystalline part of nanoparticles of the powder under investigation is 45 ± 4 nm. Magnetization J is determined using the formula J = (B/μ0)–H, where B and H are the induction and strength of the magnetic field in the sample, which are measured by the NMR method. The magnetic characteristics of MgFe2O4 are as follows: specific saturation magnetization J sat = 17.52 A m2/kg, specific residual magnetization J r = 5.73 A m2/kg, coercive force H c = 4600 A/m, and magnetic moment P sat = 371 × 10–20 A m2 in the magnetic saturation state and P r = 121 × 10–20 A m2 in the residual magnetization state.
References
L. Shekoufeh, et al., Pharmazie 67, 817 (2012).
S. Laurent, et al., Adv. Colloid Interface Sci. 166, 8 (2011).
A. Shokuhfar, et al., Nanoscale Res. Lett. 8, 540 (2013).
S. P. Gubin, et al., Usp. Khim., No. 74(6), 539 (2005).
Z. Karimi, et al., Mater. Sci. Eng. C 42, 608 (2013).
Q. A. Pankhurst, J. Connolly, S. K. Jones, and J. Dobson, J. Phys. D: Appl. Phys. 36, R167 (2003).
D. A. Baranov and S. P. Gubin, Nanosistemy 1 (1–2), 127 (2009).
M. E. Rabanal, A. Varez, B. Levenfeld, and J. M. Torralba, J. Mater. Process. Technol. 143–144, 470 (2003).
A. Zieba and S. Foner, Rev. Sci. Instrum. 53, 1344 (1982).
V. I. Nizhankovskii and I. B. Lugansky, Meas. Sci. Technol., No. 18, 1533 (2007).
V. M. Khot, A. B. Salunkhe, M. R. Phadatare, and S. H. Pawar, Mater. Chem. Phys. 132, 782 (2012).
A. I. Zhernovoi, Measuring of Magnetic Fields by Nutation Methods (Energiya, Leningrad, 1979).
A. I. Zhernovoi and S. V. D’yachenko, Tech. Phys. 60, 595 (2015).
A. I. Zhernovoi, et al., Nauchn. Priborostr. 19 (3), 57 (2009).
Ch. Ghelev, J. Phys.: Conf. Ser. 356, 012048 (2012).
A. A. Komlev and A. S. Semenova, Nanosist. Fiz. Khim. Mat. 3 (6), 105 (2012).
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Original Russian Text © A.I. Zhernovoi, A.A. Komlev, S.V. D’yachenko, 2016, published in Zhurnal Tekhnicheskoi Fiziki, 2016, Vol. 61, No. 2, pp. 146–148.
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Zhernovoi, A.I., Komlev, A.A. & D’yachenko, S.V. Magnetic characteristics of MgFe2O4 nanoparticles obtained by glycine–nitrate synthesis. Tech. Phys. 61, 302–305 (2016). https://doi.org/10.1134/S1063784216020274
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DOI: https://doi.org/10.1134/S1063784216020274